{"id":"W1983937656","doi":"10.1016/j.micromeso.2012.06.009","title":"Rapid and efficient crystallization of MIL-53(Fe) by ultrasound and microwave irradiation","year":2012,"lang":"en","type":"article","venue":"Microporous and Mesoporous Materials","topic":"Metal-Organic Frameworks: Synthesis and Applications","field":"Chemistry","cited_by":170,"is_retracted":false,"has_abstract":false,"ca_institutions":"Western University","funders":"","keywords":"Irradiation; Crystallinity; Materials science; Crystallization; Microwave irradiation; Yield (engineering); Microwave; Crystal (programming language); Chemical engineering; Composite material","routes":{"ca_aff":true,"ca_fund":false,"ca_venue":false,"about_ca":false,"invisible_to_affiliation_only":false},"retraction":null,"screen":null,"direct_labels":[],"prediction":{"model_version":"metacan-v3-hybrid-931329e0061c","candidate_categories":[],"consensus_categories":[],"category_scores_codex":[0.0001246655,0.0002046292,0.0002390175,0.000186913,0.000169067,0.0001836296,0.0001747905,0.0001711699,0.001053736],"category_scores_gemma":[0.0001594846,0.0001656817,0.000167108,0.0001536153,0.0002009541,0.0002029761,0.0002318161,0.0003084539,0.0002628516],"about_ca_system_candidate":false,"about_ca_system_consensus":false,"about_ca_system_score_codex":0.0002972548,"about_ca_system_score_gemma":0.0001851032,"about_ca_topic_candidate":false,"about_ca_topic_consensus":false,"about_ca_topic_score_codex":0.001497604,"about_ca_topic_score_gemma":0.003235057,"domain_scores_codex":[0.9999081,0.000007170893,0.000007099445,0.00001735853,0.00002375261,0.00003648215],"domain_scores_gemma":[0.9999689,0.000009026699,0.00000749674,0.000006297753,0.000004279036,0.000004013722],"domain_codex":null,"domain_gemma":null,"domain_candidate":null,"domain_consensus":null,"study_design_codex":"bench_or_experimental","study_design_gemma":"bench_or_experimental","study_design_scores_codex":[0.0000593273,0.000005808846,0.00006587074,0.0000299722,0.000001850379,0.00002899284,0.00002934246,0.0001199402,0.9972067,0.0001469813,0.00005631477,0.002248694],"study_design_scores_gemma":[0.000002907241,0.00001286881,0.000308954,0.000002053344,0.000002347922,0.00002279449,0.000005802236,0.0003501268,0.9985935,0.00001453744,0.0006816887,0.000002346787],"study_design_candidate":"bench_or_experimental","study_design_consensus":"bench_or_experimental","genre_codex":"empirical","genre_gemma":"empirical","genre_scores_codex":[0.9854466,0.001336563,0.007412183,0.00009800265,0.00002746059,0.00003553014,0.000216146,0.0003157211,0.00511181],"genre_scores_gemma":[0.9951575,0.0002648979,0.002707188,0.00001064049,0.000004708711,0.00001308394,0.00009946166,0.00003383315,0.001708632],"genre_candidate":"empirical","genre_consensus":"empirical","teacher_disagreement_score":0.001497604,"threshold_uncertainty_score":0.003525138,"prediction_status":"machine_predicted_unvalidated"},"machine_scores":{"provisional":true,"baseline":true,"maturity_gate_passed":false,"score_opus":0.008105237353242714,"score_gpt":0.2101627860112835,"score_spread":0.2020575486580408,"validation_status":"score_only:v0-immature-baseline","note":"Baseline scores from an immature model (maturity gate not passed). Scores rank; they never assert a category."}}