{"id":"W2001595317","doi":"10.1016/j.aca.2005.06.002","title":"Evaluation of slurry preparation procedures for the simultaneous determination of Hg and Se in biological samples by axial view ICP OES using on-line chemical vapor generation","year":2005,"lang":"en","type":"article","venue":"Analytica Chimica Acta","topic":"Analytical chemistry methods development","field":"Chemistry","cited_by":29,"is_retracted":false,"has_abstract":false,"ca_institutions":"","funders":"National Research Council Canada","keywords":"Chemistry; Sonication; Slurry; Aqua regia; Tetramethylammonium hydroxide; Certified reference materials; Detection limit; Analytical Chemistry (journal); Chromatography; Aqueous solution; Nuclear chemistry; Metal; Organic chemistry","routes":{"ca_aff":false,"ca_fund":true,"ca_venue":false,"about_ca":false,"invisible_to_affiliation_only":true},"retraction":null,"screen":null,"direct_labels":[],"prediction":{"model_version":"metacan-v3-hybrid-931329e0061c","candidate_categories":[],"consensus_categories":[],"category_scores_codex":[0.00196228,0.0005828069,0.0004802322,0.0002852641,0.0003039417,0.0003984453,0.0007453617,0.0005636541,0.00065255],"category_scores_gemma":[0.003591947,0.0003572997,0.000292349,0.00029705,0.0003262485,0.0004250825,0.0003247438,0.0004870352,0.0004362221],"about_ca_system_candidate":false,"about_ca_system_consensus":false,"about_ca_system_score_codex":0.0003526122,"about_ca_system_score_gemma":0.0006746228,"about_ca_topic_candidate":false,"about_ca_topic_consensus":false,"about_ca_topic_score_codex":0.001452983,"about_ca_topic_score_gemma":0.002947415,"domain_scores_codex":[0.9987702,0.0003221856,0.00009116516,0.0001479234,0.0005836855,0.00008483502],"domain_scores_gemma":[0.9986101,0.0006069568,0.0001475705,0.0001529806,0.0004461371,0.00003612076],"domain_codex":null,"domain_gemma":null,"domain_candidate":null,"domain_consensus":null,"study_design_codex":"bench_or_experimental","study_design_gemma":"bench_or_experimental","study_design_scores_codex":[0.0001765626,0.00005504248,0.0003725161,0.00009720324,0.00001318727,0.00002362627,0.0000411809,0.0001272791,0.9910408,0.00005289145,0.00005309198,0.007946561],"study_design_scores_gemma":[0.00001241664,0.0004463044,0.001179474,0.000003459657,0.0000222222,0.00008130288,0.00002142277,0.001444892,0.9958638,0.00002924831,0.0008902693,0.000005135889],"study_design_candidate":"bench_or_experimental","study_design_consensus":"bench_or_experimental","genre_codex":"empirical","genre_gemma":"methods","genre_scores_codex":[0.8486264,0.001726458,0.1465594,0.0002297895,0.0001495693,0.0005078402,0.0004288448,0.0003732149,0.001398372],"genre_scores_gemma":[0.8102799,0.002165308,0.1830842,0.0001713606,0.00005676259,0.0003843576,0.001227723,0.0001811884,0.002449252],"genre_candidate":"methods","genre_consensus":null,"teacher_disagreement_score":0.00196228,"threshold_uncertainty_score":0.01037765,"prediction_status":"machine_predicted_unvalidated"},"machine_scores":{"provisional":true,"baseline":true,"maturity_gate_passed":false,"score_opus":0.1324249944250173,"score_gpt":0.390883296106492,"score_spread":0.2584583016814747,"validation_status":"score_only:v0-immature-baseline","note":"Baseline scores from an immature model (maturity gate not passed). Scores rank; they never assert a category."}}