{"id":"W2058639042","doi":"10.4028/www.scientific.net/msf.651.37","title":"<i>In Situ</i> Diffraction Studies: Thermal Decomposition of a Natural Plumbojarosite and the Development of Rietveld-Based Data Analysis Techniques","year":2010,"lang":"en","type":"article","venue":"Materials science forum","topic":"X-ray Diffraction in Crystallography","field":"Materials Science","cited_by":10,"is_retracted":false,"has_abstract":true,"ca_institutions":"University of British Columbia","funders":"","keywords":"Diffraction; Materials science; Rietveld refinement; Diffractometer; Sample (material); Analytical Chemistry (journal); X-ray crystallography; Amorphous solid; Crystallography; Optics; Physics; Chemistry; Thermodynamics; Composite material","routes":{"ca_aff":true,"ca_fund":false,"ca_venue":false,"about_ca":false,"invisible_to_affiliation_only":false},"retraction":null,"screen":null,"direct_labels":[],"prediction":{"model_version":"metacan-v3-hybrid-931329e0061c","candidate_categories":[],"consensus_categories":[],"category_scores_codex":[0.000700063,0.0005064904,0.0009189983,0.0005052092,0.0004043327,0.0004786993,0.001022839,0.0003265351,0.003240297],"category_scores_gemma":[0.001202942,0.0004526449,0.0003593615,0.001493169,0.0006097189,0.0005147986,0.0003153214,0.001268806,0.0007786189],"about_ca_system_candidate":false,"about_ca_system_consensus":false,"about_ca_system_score_codex":0.0004375158,"about_ca_system_score_gemma":0.0004809801,"about_ca_topic_candidate":false,"about_ca_topic_consensus":false,"about_ca_topic_score_codex":0.001695513,"about_ca_topic_score_gemma":0.0038301,"domain_scores_codex":[0.9995178,0.00007408018,0.00004353646,0.0001169823,0.0002073719,0.00004036591],"domain_scores_gemma":[0.9994482,0.0001303301,0.00008559468,0.0001386115,0.0001743215,0.00002297382],"domain_codex":null,"domain_gemma":null,"domain_candidate":null,"domain_consensus":null,"study_design_codex":"bench_or_experimental","study_design_gemma":"bench_or_experimental","study_design_scores_codex":[0.00009013302,0.00003073358,0.0003536802,0.0001518927,0.00001415655,0.00008489675,0.0002035183,0.0004604693,0.9905628,0.0003072032,0.0003484085,0.007392127],"study_design_scores_gemma":[0.00000880694,0.00009491071,0.001838555,0.00000577863,0.00001525686,0.0002252456,0.0000995114,0.002318249,0.9900141,0.0001358448,0.005231709,0.00001207213],"study_design_candidate":"bench_or_experimental","study_design_consensus":"bench_or_experimental","genre_codex":"empirical","genre_gemma":"empirical","genre_scores_codex":[0.7557765,0.001449019,0.2268139,0.0004870946,0.0001085432,0.0003401684,0.004461559,0.002063012,0.008500226],"genre_scores_gemma":[0.6593309,0.0027043,0.3222677,0.0001144193,0.00002847106,0.0005329472,0.005137953,0.001276393,0.008606843],"genre_candidate":"empirical","genre_consensus":"empirical","teacher_disagreement_score":0.003240297,"threshold_uncertainty_score":0.01083982,"prediction_status":"machine_predicted_unvalidated"},"machine_scores":{"provisional":true,"baseline":true,"maturity_gate_passed":false,"score_opus":0.01602474944079514,"score_gpt":0.3017219458592746,"score_spread":0.2856971964184795,"validation_status":"score_only:v0-immature-baseline","note":"Baseline scores from an immature model (maturity gate not passed). Scores rank; they never assert a category."}}