{"id":"W2120072163","doi":"10.1039/c2sc20344h","title":"Accelerated aging: a low energy, solvent-free alternative to solvothermal and mechanochemical synthesis of metal–organic materials","year":2012,"lang":"en","type":"article","venue":"Chemical Science","topic":"Metal-Organic Frameworks: Synthesis and Applications","field":"Chemistry","cited_by":217,"is_retracted":false,"has_abstract":true,"ca_institutions":"McGill University; Bruker (Canada); Centre in Green Chemistry and Catalysis","funders":"","keywords":"Materials science; Mechanochemistry; Solvothermal synthesis; Solvent; Metal; Chemical engineering; Nanotechnology; Organic chemistry; Chemistry; Inorganic chemistry; Metallurgy","routes":{"ca_aff":true,"ca_fund":false,"ca_venue":false,"about_ca":false,"invisible_to_affiliation_only":false},"retraction":null,"screen":null,"direct_labels":[],"prediction":{"model_version":"codex-gemma-dda1882f352a","candidate_categories":["insufficient_payload"],"consensus_categories":[],"category_scores_codex":[0.0004545606,0.000226057,0.0003756532,0.00006267925,0.0001108719,0.00007525027,0.00108673,0.0001443365,0.002694545],"category_scores_gemma":[0.001189125,0.000193183,0.00005965851,0.000518334,0.0004691671,0.0002396971,0.000649209,0.0001213124,0.00002248924],"about_ca_system_candidate":false,"about_ca_system_consensus":false,"about_ca_system_score_codex":0.00008364464,"about_ca_system_score_gemma":0.00006228884,"about_ca_topic_candidate":false,"about_ca_topic_consensus":false,"about_ca_topic_score_codex":0.00003429386,"about_ca_topic_score_gemma":5.522358e-7,"domain_scores_codex":[0.9980553,0.00001667432,0.000388867,0.0004986965,0.0004586268,0.0005817939],"domain_scores_gemma":[0.9983786,0.0002430927,0.0001699805,0.0006640362,0.0001071408,0.0004371706],"domain_codex":null,"domain_gemma":null,"domain_candidate":null,"domain_consensus":null,"study_design_codex":"bench_or_experimental","study_design_gemma":"bench_or_experimental","study_design_scores_codex":[0.00001027703,0.0001403633,0.0000324413,0.00003440526,0.00002192039,3.415713e-7,0.0001204509,2.902248e-7,0.9954034,0.00261234,0.0001015245,0.001522207],"study_design_scores_gemma":[0.0001075419,0.000004074484,0.00002602948,0.0000913469,0.00004137676,0.000007216854,0.00006294055,0.00008580941,0.9984171,0.0007031391,0.0002255178,0.0002279074],"study_design_candidate":"bench_or_experimental","study_design_consensus":"bench_or_experimental","genre_codex":"empirical","genre_gemma":"empirical","genre_scores_codex":[0.9966807,0.0001297257,0.00108786,0.0004230182,0.00006702049,0.00006884155,0.00004601144,0.00005302181,0.00144382],"genre_scores_gemma":[0.9964939,0.00002456924,0.00295369,0.0001275457,0.0002021938,0.00007751723,0.000004015727,0.00002627809,0.00009028999],"genre_candidate":"empirical","genre_consensus":"empirical","teacher_disagreement_score":0.003013661,"threshold_uncertainty_score":0.9982171,"prediction_status":"machine_predicted_unvalidated"},"machine_scores":{"provisional":true,"baseline":true,"maturity_gate_passed":false,"score_opus":0.02025074209256891,"score_gpt":0.2554762917725865,"score_spread":0.2352255496800175,"validation_status":"score_only:v0-immature-baseline","note":"Baseline scores from an immature model (maturity gate not passed). Scores rank; they never assert a category."}}