{"id":"W2120072163","doi":"10.1039/c2sc20344h","title":"Accelerated aging: a low energy, solvent-free alternative to solvothermal and mechanochemical synthesis of metal–organic materials","year":2012,"lang":"en","type":"article","venue":"Chemical Science","topic":"Metal-Organic Frameworks: Synthesis and Applications","field":"Chemistry","cited_by":217,"is_retracted":false,"has_abstract":true,"ca_institutions":"McGill University; Bruker (Canada); Centre in Green Chemistry and Catalysis","funders":"","keywords":"Materials science; Mechanochemistry; Solvothermal synthesis; Solvent; Metal; Chemical engineering; Nanotechnology; Organic chemistry; Chemistry; Inorganic chemistry; Metallurgy","routes":{"ca_aff":true,"ca_fund":false,"ca_venue":false,"about_ca":false,"invisible_to_affiliation_only":false},"retraction":null,"screen":null,"direct_labels":[],"prediction":{"model_version":"metacan-v3-hybrid-931329e0061c","candidate_categories":[],"consensus_categories":[],"category_scores_codex":[0.0002557944,0.0003444893,0.0002319992,0.0002342341,0.0002315519,0.0002729336,0.0005345163,0.0003347209,0.0009404952],"category_scores_gemma":[0.0001561128,0.0001687264,0.0002692357,0.00013427,0.0002443544,0.0006211095,0.0004219937,0.0005696915,0.0002929449],"about_ca_system_candidate":false,"about_ca_system_consensus":false,"about_ca_system_score_codex":0.0002111428,"about_ca_system_score_gemma":0.0002815934,"about_ca_topic_candidate":false,"about_ca_topic_consensus":false,"about_ca_topic_score_codex":0.0001654029,"about_ca_topic_score_gemma":0.0004791867,"domain_scores_codex":[0.9998509,0.00002079882,0.000008507415,0.00003364254,0.00005477695,0.00003133217],"domain_scores_gemma":[0.9999082,0.00001762597,0.0000319287,0.00001919477,0.00001279817,0.0000103167],"domain_codex":null,"domain_gemma":null,"domain_candidate":null,"domain_consensus":null,"study_design_codex":"bench_or_experimental","study_design_gemma":"bench_or_experimental","study_design_scores_codex":[0.00005655631,0.00005280871,0.0001411804,0.0001665043,0.00001163623,0.0001549053,0.00005401243,0.0005409886,0.9736075,0.004447991,0.0003444094,0.02042155],"study_design_scores_gemma":[0.00001189824,0.0002096104,0.0002295729,0.000005233091,0.000008096185,0.0002667108,0.000008635614,0.002213913,0.9880413,0.0004046362,0.00858891,0.00001154885],"study_design_candidate":"bench_or_experimental","study_design_consensus":"bench_or_experimental","genre_codex":"empirical","genre_gemma":"empirical","genre_scores_codex":[0.7783672,0.01121829,0.1967399,0.0007249124,0.0004082621,0.0001634394,0.0001909666,0.000911289,0.01127581],"genre_scores_gemma":[0.9171267,0.003642117,0.07345971,0.0002816945,0.00017246,0.00007988715,0.0001455108,0.00009571996,0.004996234],"genre_candidate":"empirical","genre_consensus":"empirical","teacher_disagreement_score":0.0009404952,"threshold_uncertainty_score":0.003146291,"prediction_status":"machine_predicted_unvalidated"},"machine_scores":{"provisional":true,"baseline":true,"maturity_gate_passed":false,"score_opus":0.02025074209256891,"score_gpt":0.2554762917725865,"score_spread":0.2352255496800175,"validation_status":"score_only:v0-immature-baseline","note":"Baseline scores from an immature model (maturity gate not passed). Scores rank; they never assert a category."}}