{"id":"W2603328630","doi":"10.1007/s10904-017-0528-6","title":"Ultrasound-Assisted Synthesis of Novel Nano 3D Supramolecular Lead(II) Metal–Organic Coordination System: A New Precursor to Produce Nano Lead Oxide","year":2017,"lang":"en","type":"article","venue":"Journal of Inorganic and Organometallic Polymers and Materials","topic":"Metal-Organic Frameworks: Synthesis and Applications","field":"Chemistry","cited_by":3,"is_retracted":false,"has_abstract":false,"ca_institutions":"University of Waterloo","funders":"University of Waterloo; National Research Foundation of Korea","keywords":"Hexamethylenetetramine; Thermogravimetric analysis; Supramolecular chemistry; Lead oxide; Nanoparticle; Thermal decomposition; Coordination number; Nanorod; Materials science; Scanning electron microscope; Nano-; Coordination complex; Oxide; Metal; Crystal structure; Inorganic chemistry; Chemistry; Crystallography; Nanotechnology; Ion; Organic chemistry","routes":{"ca_aff":true,"ca_fund":true,"ca_venue":false,"about_ca":false,"invisible_to_affiliation_only":false},"retraction":null,"screen":null,"direct_labels":[],"prediction":{"model_version":"codex-gemma-dda1882f352a","candidate_categories":["metaepi_narrow","insufficient_payload"],"consensus_categories":[],"category_scores_codex":[0.0008745581,0.0004608577,0.00132532,0.0002305697,0.0005659024,0.0003480301,0.000746242,0.0003082769,0.001382024],"category_scores_gemma":[0.001733652,0.0003829562,0.0001699764,0.0002463789,0.0002220271,0.0004157673,0.0002651489,0.000182884,0.00001309453],"about_ca_system_candidate":false,"about_ca_system_consensus":false,"about_ca_system_score_codex":0.0001019243,"about_ca_system_score_gemma":0.000276085,"about_ca_topic_candidate":false,"about_ca_topic_consensus":false,"about_ca_topic_score_codex":0.0001744119,"about_ca_topic_score_gemma":0.00001020423,"domain_scores_codex":[0.9971457,0.00007500783,0.001371208,0.0005201201,0.0004614019,0.0004265239],"domain_scores_gemma":[0.9962879,0.0002285295,0.00200771,0.0008615956,0.0002409265,0.0003733485],"domain_codex":null,"domain_gemma":null,"domain_candidate":null,"domain_consensus":null,"study_design_codex":"bench_or_experimental","study_design_gemma":"bench_or_experimental","study_design_scores_codex":[0.00008864323,0.000242373,0.00005889878,0.0004081126,0.0005031031,0.000005314642,0.000275734,2.378884e-7,0.9945586,0.0005691166,0.0001789301,0.003110955],"study_design_scores_gemma":[0.0007745997,0.0001023829,0.001139934,0.0005667712,0.0009022876,0.0007512239,0.0005937476,0.000002446053,0.9938722,0.00003441754,0.0008641492,0.0003957899],"study_design_candidate":"bench_or_experimental","study_design_consensus":"bench_or_experimental","genre_codex":"empirical","genre_gemma":"empirical","genre_scores_codex":[0.993898,0.001851318,0.002248658,0.0009243026,0.0002929252,0.0002653189,0.0001054151,0.00003361234,0.0003804774],"genre_scores_gemma":[0.9927069,0.0004627365,0.004140032,0.00006420246,0.0002870007,0.00001577608,0.000007080716,0.00009128414,0.002224972],"genre_candidate":"empirical","genre_consensus":"empirical","teacher_disagreement_score":0.002715165,"threshold_uncertainty_score":0.9998623,"prediction_status":"machine_predicted_unvalidated"},"machine_scores":{"provisional":true,"baseline":true,"maturity_gate_passed":false,"score_opus":0.01535290896811736,"score_gpt":0.2367730311738671,"score_spread":0.2214201222057497,"validation_status":"score_only:v0-immature-baseline","note":"Baseline scores from an immature model (maturity gate not passed). Scores rank; they never assert a category."}}