{"id":"W2762630560","doi":"10.1007/s12678-017-0426-2","title":"Design and Development of Instrumentations for the Preparation of Platinum Single Crystals for Electrochemistry and Electrocatalysis Research Part 3: Final Treatment, Electrochemical Measurements, and Recommended Laboratory Practices","year":2017,"lang":"en","type":"article","venue":"Electrocatalysis","topic":"Electrochemical Analysis and Applications","field":"Chemistry","cited_by":38,"is_retracted":false,"has_abstract":false,"ca_institutions":"Queen's University","funders":"","keywords":"Electrocatalyst; Electrochemistry; Platinum; Materials science; Annealing (glass); Electrode; Electrolyte; Chemical engineering; Monocrystalline silicon; Nanotechnology; Electrochemical cell; Oxide; Catalysis; Metallurgy; Chemistry; Silicon; Organic chemistry; Engineering","routes":{"ca_aff":true,"ca_fund":false,"ca_venue":false,"about_ca":false,"invisible_to_affiliation_only":false},"retraction":null,"screen":null,"direct_labels":[],"prediction":{"model_version":"metacan-v3-hybrid-931329e0061c","candidate_categories":[],"consensus_categories":[],"category_scores_codex":[0.003485892,0.001371858,0.001354733,0.001601824,0.001446678,0.001071709,0.003105837,0.001361093,0.008867448],"category_scores_gemma":[0.00398266,0.001440171,0.0006869717,0.001279273,0.0007803887,0.001067021,0.0008380737,0.002077323,0.008305788],"about_ca_system_candidate":false,"about_ca_system_consensus":false,"about_ca_system_score_codex":0.001345086,"about_ca_system_score_gemma":0.004621961,"about_ca_topic_candidate":false,"about_ca_topic_consensus":false,"about_ca_topic_score_codex":0.001551475,"about_ca_topic_score_gemma":0.003487415,"domain_scores_codex":[0.9974906,0.0002020798,0.0002020222,0.0004872627,0.001445724,0.0001722796],"domain_scores_gemma":[0.9959416,0.0004882892,0.0003465689,0.0009186538,0.002064472,0.0002403438],"domain_codex":null,"domain_gemma":null,"domain_candidate":null,"domain_consensus":null,"study_design_codex":"bench_or_experimental","study_design_gemma":"bench_or_experimental","study_design_scores_codex":[0.0002371704,0.0001826329,0.001539592,0.0004819371,0.00003203126,0.00006699398,0.0001539029,0.001154723,0.8982681,0.002806825,0.006728348,0.0883477],"study_design_scores_gemma":[0.00004681016,0.0003727651,0.002267763,0.00002206162,0.00003055308,0.0001266224,0.00003514087,0.004910382,0.9570728,0.0005572228,0.03452059,0.00003722836],"study_design_candidate":"bench_or_experimental","study_design_consensus":"bench_or_experimental","genre_codex":"methods","genre_gemma":"methods","genre_scores_codex":[0.03184499,0.0006225466,0.9445354,0.0005437025,0.0004014788,0.005071079,0.004003608,0.006998102,0.005978971],"genre_scores_gemma":[0.05850031,0.0009718036,0.9192863,0.0003389406,0.0001070229,0.005749255,0.004823782,0.001014419,0.009208168],"genre_candidate":"methods","genre_consensus":"methods","teacher_disagreement_score":0.008867448,"threshold_uncertainty_score":0.02966458,"prediction_status":"machine_predicted_unvalidated"},"machine_scores":{"provisional":true,"baseline":true,"maturity_gate_passed":false,"score_opus":0.2121354709611377,"score_gpt":0.4050368025737223,"score_spread":0.1929013316125846,"validation_status":"score_only:v0-immature-baseline","note":"Baseline scores from an immature model (maturity gate not passed). Scores rank; they never assert a category."}}