{"id":"W2950443817","doi":"10.1021/ic100062x","title":"Syntheses, Raman Spectra, and X-ray Crystal Structures of [XeF<sub>5</sub>][μ-F(OsO<sub>3</sub>F<sub>2</sub>)<sub>2</sub>] and [M][OsO<sub>3</sub>F<sub>3</sub>] (M = XeF<sub>5</sub><sup>+</sup>, Xe<sub>2</sub>F<sub>11</sub><sup>+</sup>)","year":2010,"lang":"en","type":"article","venue":"Inorganic Chemistry","topic":"Inorganic Fluorides and Related Compounds","field":"Chemistry","cited_by":22,"is_retracted":false,"has_abstract":true,"ca_institutions":"McMaster University","funders":"","keywords":"Chemistry; Crystallography; Fluorine; Crystal structure; Octahedron; Oxide; Raman spectroscopy; Metal; Fluoride; X-ray crystallography; Inorganic chemistry","routes":{"ca_aff":true,"ca_fund":false,"ca_venue":false,"about_ca":false,"invisible_to_affiliation_only":false},"retraction":null,"screen":null,"direct_labels":[],"prediction":{"model_version":"codex-gemma-dda1882f352a","candidate_categories":["metaepi_narrow","sts","scholarly_communication","open_science","research_integrity","insufficient_payload"],"consensus_categories":["metaepi_narrow","sts","research_integrity"],"category_scores_codex":[0.005614189,0.01527577,0.01304478,0.00345008,0.006271147,0.004593764,0.01084636,0.01579374,0.0007117975],"category_scores_gemma":[0.005087785,0.01695214,0.006168027,0.008750218,0.008718985,0.004906553,0.007588093,0.02210904,0.001744231],"about_ca_system_candidate":true,"about_ca_system_consensus":true,"about_ca_system_score_codex":0.00587217,"about_ca_system_score_gemma":0.006516754,"about_ca_topic_candidate":false,"about_ca_topic_consensus":false,"about_ca_topic_score_codex":0.0003440922,"about_ca_topic_score_gemma":0.001145292,"domain_scores_codex":[0.9422078,0.001983171,0.01406766,0.01606519,0.0104706,0.01520566],"domain_scores_gemma":[0.9583425,0.005256855,0.008845639,0.01428965,0.004389268,0.008876073],"domain_codex":null,"domain_gemma":null,"domain_candidate":null,"domain_consensus":null,"study_design_codex":"bench_or_experimental","study_design_gemma":"bench_or_experimental","study_design_scores_codex":[0.003122918,0.004094485,0.002424185,0.007621586,0.006319578,0.003339768,0.003966616,0.001383799,0.9295467,0.0004139469,0.01699225,0.02077424],"study_design_scores_gemma":[0.01583823,0.001238737,0.001748522,0.004624863,0.005977341,0.008039936,0.004061954,0.003586723,0.9326332,0.003037017,0.00259107,0.01662244],"study_design_candidate":"bench_or_experimental","study_design_consensus":"bench_or_experimental","genre_codex":"empirical","genre_gemma":"empirical","genre_scores_codex":[0.965888,0.008791032,0.0003734976,0.001624754,0.004701748,0.005654539,0.005385056,0.004906218,0.002675151],"genre_scores_gemma":[0.9599186,0.01614899,0.0004415117,0.001544556,0.01094396,0.00125699,0.004527851,0.005075143,0.0001424637],"genre_candidate":"empirical","genre_consensus":"empirical","teacher_disagreement_score":0.01613479,"threshold_uncertainty_score":0.9991153,"prediction_status":"machine_predicted_unvalidated"},"machine_scores":{"provisional":true,"baseline":true,"maturity_gate_passed":false,"score_opus":0.005228154280727109,"score_gpt":0.1903060676721783,"score_spread":0.1850779133914512,"validation_status":"score_only:v0-immature-baseline","note":"Baseline scores from an immature model (maturity gate not passed). Scores rank; they never assert a category."}}