{"id":"W2953213892","doi":"10.1021/cm501862u","title":"Solid-State <sup>69</sup>Ga and <sup>71</sup>Ga NMR Study of the Nanoscale Inorganic Cluster [Ga<sub>13</sub>(μ<sub>3</sub>-OH)<sub>6</sub>(μ<sub>2</sub>-OH)<sub>18</sub>(H<sub>2</sub>O)<sub>24</sub>](NO<sub>3</sub>)<sub>15</sub>","year":2014,"lang":"en","type":"article","venue":"Chemistry of Materials","topic":"Advanced NMR Techniques and Applications","field":"Chemistry","cited_by":11,"is_retracted":false,"has_abstract":true,"ca_institutions":"University of Ottawa","funders":"Division of Chemistry; Fonds National de la Recherche Luxembourg; National Science Foundation","keywords":"Gallium; Octahedron; Solid-state nuclear magnetic resonance; Crystallography; Cluster (spacecraft); Materials science; NMR spectra database; Solid-state; Crystal structure; Chemistry; Nuclear magnetic resonance; Physical chemistry; Spectral line; Physics","routes":{"ca_aff":true,"ca_fund":false,"ca_venue":false,"about_ca":false,"invisible_to_affiliation_only":false},"retraction":null,"screen":null,"direct_labels":[],"prediction":{"model_version":"codex-gemma-dda1882f352a","candidate_categories":["metaepi_narrow","sts","scholarly_communication","open_science","research_integrity","insufficient_payload"],"consensus_categories":["metaepi_narrow","sts","research_integrity"],"category_scores_codex":[0.006482674,0.01047673,0.01178496,0.00178043,0.004349509,0.002265609,0.009432393,0.00716644,0.000334425],"category_scores_gemma":[0.003154542,0.01095554,0.00410834,0.005217442,0.005476475,0.003528554,0.007412043,0.007136151,0.001873732],"about_ca_system_candidate":false,"about_ca_system_consensus":false,"about_ca_system_score_codex":0.003407977,"about_ca_system_score_gemma":0.002489505,"about_ca_topic_candidate":false,"about_ca_topic_consensus":false,"about_ca_topic_score_codex":0.0001438508,"about_ca_topic_score_gemma":0.0003673964,"domain_scores_codex":[0.9543119,0.002596631,0.01395172,0.0117103,0.007209192,0.01022026],"domain_scores_gemma":[0.9638337,0.002989071,0.01068039,0.01355203,0.004220972,0.0047238],"domain_codex":null,"domain_gemma":null,"domain_candidate":null,"domain_consensus":null,"study_design_codex":"bench_or_experimental","study_design_gemma":"bench_or_experimental","study_design_scores_codex":[0.002695877,0.005685061,0.0007305375,0.008224411,0.002335029,0.0003718858,0.002650686,0.002581112,0.944266,0.0000814335,0.01651086,0.01386708],"study_design_scores_gemma":[0.01327134,0.001259064,0.001006842,0.003977692,0.003274276,0.001215423,0.002335776,0.001530755,0.9565699,0.002822126,0.002489136,0.01024764],"study_design_candidate":"bench_or_experimental","study_design_consensus":"bench_or_experimental","genre_codex":"empirical","genre_gemma":"empirical","genre_scores_codex":[0.9730668,0.001810413,0.001247897,0.001150908,0.001712582,0.009756995,0.006351399,0.003735622,0.001167377],"genre_scores_gemma":[0.9694213,0.01042451,0.0006085886,0.001752299,0.0046087,0.005967471,0.003668887,0.003381508,0.0001667783],"genre_candidate":"empirical","genre_consensus":"empirical","teacher_disagreement_score":0.01402173,"threshold_uncertainty_score":0.9989035,"prediction_status":"machine_predicted_unvalidated"},"machine_scores":{"provisional":true,"baseline":true,"maturity_gate_passed":false,"score_opus":0.009666830452895991,"score_gpt":0.2410173109734977,"score_spread":0.2313504805206018,"validation_status":"score_only:v0-immature-baseline","note":"Baseline scores from an immature model (maturity gate not passed). Scores rank; they never assert a category."}}