{"id":"W2990832532","doi":"10.1007/s12127-019-00253-z","title":"Determination of ethambutol in biological samples using graphene oxide based dispersive solid-phase microextraction followed by ion mobility spectrometry","year":2019,"lang":"en","type":"article","venue":"International Journal for Ion Mobility Spectrometry","topic":"Analytical chemistry methods development","field":"Chemistry","cited_by":11,"is_retracted":false,"has_abstract":false,"ca_institutions":"Cape Breton University","funders":"Damghan University","keywords":"Ion-mobility spectrometry; Detection limit; Solid-phase microextraction; Chromatography; Calibration curve; Graphene; Chemistry; Materials science; Analytical Chemistry (journal); Mass spectrometry; Ethambutol; Gas chromatography–mass spectrometry; Nanotechnology","routes":{"ca_aff":true,"ca_fund":false,"ca_venue":false,"about_ca":false,"invisible_to_affiliation_only":false},"retraction":null,"screen":null,"direct_labels":[],"prediction":{"model_version":"codex-gemma-dda1882f352a","candidate_categories":["metaepi_narrow","insufficient_payload"],"consensus_categories":[],"category_scores_codex":[0.001590566,0.0003911074,0.0006712647,0.0005788655,0.00009617859,0.00009198459,0.0006454657,0.0003872725,0.001698388],"category_scores_gemma":[0.001810219,0.0003789613,0.0005990671,0.0005380685,0.0001734054,0.0004218537,0.0001063861,0.0007708127,0.000005204608],"about_ca_system_candidate":false,"about_ca_system_consensus":false,"about_ca_system_score_codex":0.002243889,"about_ca_system_score_gemma":0.0002173282,"about_ca_topic_candidate":false,"about_ca_topic_consensus":false,"about_ca_topic_score_codex":0.00007147097,"about_ca_topic_score_gemma":0.000009255843,"domain_scores_codex":[0.9962466,0.0001519292,0.001414877,0.0007625386,0.0009110764,0.0005129358],"domain_scores_gemma":[0.9967351,0.001195173,0.0008698326,0.0003777458,0.0006119252,0.0002102211],"domain_codex":null,"domain_gemma":null,"domain_candidate":null,"domain_consensus":null,"study_design_codex":"bench_or_experimental","study_design_gemma":"bench_or_experimental","study_design_scores_codex":[0.001193828,0.001696112,0.03413241,0.000126994,0.0001311108,0.00001493205,0.0000358959,0.00008963108,0.9616191,0.000066502,0.00001969525,0.000873834],"study_design_scores_gemma":[0.003679504,0.000216267,0.00768804,0.0001654441,0.00005326702,0.000112653,0.0003989316,0.00844291,0.9752786,0.003336324,0.0002249836,0.0004030893],"study_design_candidate":"bench_or_experimental","study_design_consensus":"bench_or_experimental","genre_codex":"empirical","genre_gemma":"empirical","genre_scores_codex":[0.7851612,0.00009180555,0.2134632,0.0001449918,0.000470432,0.0002769803,0.000246536,0.00002999393,0.0001148917],"genre_scores_gemma":[0.9322006,0.00004332944,0.06716512,0.00004860579,0.0001827986,0.00002188138,0.0002395576,0.00003039641,0.00006770021],"genre_candidate":"empirical","genre_consensus":"empirical","teacher_disagreement_score":0.1470394,"threshold_uncertainty_score":0.9998662,"prediction_status":"machine_predicted_unvalidated"},"machine_scores":{"provisional":true,"baseline":true,"maturity_gate_passed":false,"score_opus":0.04078174653209998,"score_gpt":0.3848172812023629,"score_spread":0.3440355346702629,"validation_status":"score_only:v0-immature-baseline","note":"Baseline scores from an immature model (maturity gate not passed). Scores rank; they never assert a category."}}