{"id":"W4293102207","doi":"10.1002/anie.202207206","title":"High‐Humidity Shaker Aging to Access Chitin and Cellulose Nanocrystals**","year":2022,"lang":"en","type":"article","venue":"Angewandte Chemie International Edition","topic":"Advanced Cellulose Research Studies","field":"Materials Science","cited_by":25,"is_retracted":false,"has_abstract":true,"ca_institutions":"National Research Council Canada; McGill University","funders":"Fonds de recherche du Québec – Nature et technologies; National Research Council Canada; Canada Foundation for Innovation; McGill University; Centre in Green Chemistry and Catalysis; Natural Sciences and Engineering Research Council of Canada","keywords":"Cellulose; Nanocrystalline material; Chitin; Chemical engineering; Ammonium persulfate; Aqueous solution; Solvent; Humidity; Chemistry; Supramolecular chemistry; Materials science; Nanocellulose; Pulp (tooth); Nanotechnology; Organic chemistry; Chitosan; Polymer; Molecule","routes":{"ca_aff":true,"ca_fund":true,"ca_venue":false,"about_ca":false,"invisible_to_affiliation_only":false},"retraction":null,"screen":null,"direct_labels":[],"prediction":{"model_version":"codex-gemma-dda1882f352a","candidate_categories":["insufficient_payload"],"consensus_categories":[],"category_scores_codex":[0.0003926524,0.000144002,0.0001488448,0.0001275675,0.000357326,0.0001527276,0.0003980068,0.00002431263,0.004210464],"category_scores_gemma":[0.0001982641,0.0001484617,0.0000393097,0.0001651912,0.00008699035,0.0005301527,0.001136331,0.0001745509,0.00004605727],"about_ca_system_candidate":false,"about_ca_system_consensus":false,"about_ca_system_score_codex":0.0003016196,"about_ca_system_score_gemma":0.00003494884,"about_ca_topic_candidate":false,"about_ca_topic_consensus":false,"about_ca_topic_score_codex":0.0001201923,"about_ca_topic_score_gemma":0.00001493137,"domain_scores_codex":[0.9982755,0.0000462778,0.0002177505,0.0004207694,0.000747613,0.000292044],"domain_scores_gemma":[0.999358,0.0001281406,0.00009854182,0.0001480925,0.0001501028,0.0001170984],"domain_codex":null,"domain_gemma":null,"domain_candidate":null,"domain_consensus":null,"study_design_codex":"bench_or_experimental","study_design_gemma":"bench_or_experimental","study_design_scores_codex":[0.00005515557,0.00006700098,0.0001968978,0.00002289539,0.00001518576,0.00003203742,0.0002577353,0.000244481,0.9802139,0.0005721326,0.0177091,0.0006134573],"study_design_scores_gemma":[0.0003107532,0.00004197752,0.0009298046,0.00001914835,0.000006124874,0.00001700532,0.0001693549,0.00002998557,0.962163,0.002764097,0.03338305,0.0001656432],"study_design_candidate":"bench_or_experimental","study_design_consensus":"bench_or_experimental","genre_codex":"empirical","genre_gemma":"empirical","genre_scores_codex":[0.9819375,0.0001961331,0.005942426,0.005333278,0.002240977,0.0002938,0.000551177,0.000129984,0.00337468],"genre_scores_gemma":[0.9957257,0.00006345679,0.000769295,0.0005526522,0.001018076,0.0002449686,0.0002380645,0.00001876897,0.001369022],"genre_candidate":"empirical","genre_consensus":"empirical","teacher_disagreement_score":0.01805087,"threshold_uncertainty_score":0.9966998,"prediction_status":"machine_predicted_unvalidated"},"machine_scores":{"provisional":true,"baseline":true,"maturity_gate_passed":false,"score_opus":0.02693836230702227,"score_gpt":0.3122241986068676,"score_spread":0.2852858362998453,"validation_status":"score_only:v0-immature-baseline","note":"Baseline scores from an immature model (maturity gate not passed). Scores rank; they never assert a category."}}