{"id":"W4399363080","doi":"10.1021/acscatal.4c01447","title":"A Universal Roadmap for Quantification of Glycerol Electrooxidation Products Using Proton Nuclear Magnetic Spectroscopy (<sup>1</sup>H NMR)","year":2024,"lang":"en","type":"article","venue":"ACS Catalysis","topic":"CO2 Reduction Techniques and Catalysts","field":"Energy","cited_by":38,"is_retracted":false,"has_abstract":true,"ca_institutions":"McMaster University","funders":"Natural Sciences and Engineering Research Council of Canada","keywords":"Glycerol; Chemistry; Proton NMR; Nuclear magnetic resonance spectroscopy; Catalysis; Organic chemistry","routes":{"ca_aff":true,"ca_fund":true,"ca_venue":false,"about_ca":false,"invisible_to_affiliation_only":false},"retraction":null,"screen":null,"direct_labels":[],"prediction":{"model_version":"metacan-v3-hybrid-931329e0061c","candidate_categories":[],"consensus_categories":[],"category_scores_codex":[0.004014083,0.00276402,0.001123547,0.001686764,0.0006048564,0.002252398,0.00251878,0.002824632,0.005265271],"category_scores_gemma":[0.004123083,0.0009906791,0.0006681294,0.0009554274,0.001770435,0.003418676,0.002143226,0.003109872,0.004562678],"about_ca_system_candidate":false,"about_ca_system_consensus":false,"about_ca_system_score_codex":0.0009862484,"about_ca_system_score_gemma":0.001393277,"about_ca_topic_candidate":false,"about_ca_topic_consensus":false,"about_ca_topic_score_codex":0.0006489454,"about_ca_topic_score_gemma":0.001120985,"domain_scores_codex":[0.9978172,0.0004812474,0.000121291,0.0005009801,0.000960543,0.0001187405],"domain_scores_gemma":[0.9973609,0.0006003639,0.0003473888,0.0002771202,0.001269717,0.0001445235],"domain_codex":null,"domain_gemma":null,"domain_candidate":null,"domain_consensus":null,"study_design_codex":"bench_or_experimental","study_design_gemma":"bench_or_experimental","study_design_scores_codex":[0.0002217571,0.000111663,0.001085619,0.0009039649,0.00004419584,0.0001804454,0.00008118578,0.001753287,0.8746815,0.008180252,0.006131975,0.106624],"study_design_scores_gemma":[0.00002009765,0.0004034959,0.001057595,0.0002093524,0.00006638183,0.0004517067,0.0001436073,0.009473196,0.9282008,0.005897777,0.05399693,0.00007901478],"study_design_candidate":"bench_or_experimental","study_design_consensus":"bench_or_experimental","genre_codex":"methods","genre_gemma":"methods","genre_scores_codex":[0.01827198,0.01329025,0.9441448,0.004244844,0.0008782785,0.0006471183,0.002782717,0.006819272,0.008920685],"genre_scores_gemma":[0.06958915,0.01013442,0.9081882,0.002032969,0.0002303045,0.001227907,0.002843799,0.0005054984,0.005247814],"genre_candidate":"methods","genre_consensus":"methods","teacher_disagreement_score":0.005265271,"threshold_uncertainty_score":0.02122879,"prediction_status":"machine_predicted_unvalidated"},"machine_scores":{"provisional":true,"baseline":true,"maturity_gate_passed":false,"score_opus":0.01541107888258154,"score_gpt":0.2610366021584205,"score_spread":0.245625523275839,"validation_status":"score_only:v0-immature-baseline","note":"Baseline scores from an immature model (maturity gate not passed). Scores rank; they never assert a category."}}