<i>IN‐SITU</i>MICROWAVE‐ASSISTED FABRICATION OF POLYMERIC NANOCOMPOSITES
Bibliographic record
Abstract
Gold – poly(dimethylsiloxane) (Au–PDMS) nanocomposites are synthesized in the form of gels, foams, and films. In this chapter, the authors report their results on a novel in situ synthesis of Au–PDMS by using a microwave-induced reduction of gold ions. Microwave heating has been studied as a promising technique for nanoparticle synthesis. Microwave irradiation has been used for the preparation of gold and silver nanoparticles under various conditions. The authors investigate the microwave-induced reduction of gold ions onto a PDMS matrix and the usefulness of the nanocomposite for sensing application. During the interaction between PDMS and the solution, sub-nanometer- sized gold seeds are formed on the surface, which possibly initiate the formation of gold nanoparticles during the irradiation. The gold nanoparticles prepared by microwave irradiation are distributed in the polymer matrix, and to increase the density of nanoparticles on the surface, an annealing process is employed.
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How this classification was reachedexpand
Full frame machine prediction
Teacher imitationNot calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.
Distilled classifier scores by category (both heads)
| Category | Codex | Gemma |
|---|---|---|
| Metaresearch | 0.000 | 0.000 |
| Meta-epidemiology (narrow) | 0.000 | 0.000 |
| Meta-epidemiology (broad) | 0.000 | 0.000 |
| Bibliometrics | 0.000 | 0.000 |
| Science and technology studies | 0.000 | 0.000 |
| Scholarly communication | 0.000 | 0.000 |
| Open science | 0.000 | 0.000 |
| Research integrity | 0.000 | 0.000 |
| Insufficient payload (model declined to judge) | 0.002 | 0.000 |
Machine scores (provisional)
The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.
Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.
score_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from itClassification
machine, unvalidatedMachine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.
How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".