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Record W2054238633 · doi:10.1021/ie901795e

CO<sub>2</sub> Carrying Behavior of Calcium Aluminate Pellets under High-Temperature/High-CO<sub>2</sub> Concentration Calcination Conditions

2010· article· en· W2054238633 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.

Bibliographic record

VenueIndustrial & Engineering Chemistry Research · 2010
Typearticle
Languageen
FieldEngineering
TopicChemical Looping and Thermochemical Processes
Canadian institutionsNatural Resources Canada
Fundersnot available
KeywordsCalcinationCarbonationSorbentPelletsSinteringCalcium loopingMaterials scienceAluminateChemical engineeringThermogravimetric analysisDiffusionMineralogyMetallurgyCementChemistryComposite materialAdsorptionCatalysisThermodynamics

Abstract

fetched live from OpenAlex

Sintering and a resulting loss of activity during calcination/carbonation can introduce substantial economic penalties for a CO 2 looping cycle using CaO-based sorbents. In a real system, sorbent regeneration must be done at a high temperature to produce an almost pure CO 2 stream, and this will increase both sintering and loss of sorbent activity. The influence of severe calcination conditions on the CO 2 carrying behavior of calcium aluminate pellets is investigated here. Up to 30 calcination/carbonation cycles were performed using a thermogravimetric analyzer apparatus. The maximum temperature during the calcination stage in pure CO 2 was 950 °C, using different heating/cooling rates between two carbonation stages (700 °C, 20% CO 2 ). For comparison, cycles were also done using N 2 during the calcination stages. In addition, the original Cadomin limestone, used for pelletization, was also examined in its original form and the results obtained were compared with those for the aluminate pellets. As expected, high temperature during calcination strongly reduced CO 2 carrying capacities of both sorbents. However, aluminate pellets showed better resistance to these severe conditions. The conversion profiles obtained are significantly different to those obtained under milder conditions, with significant increased activity during the slower, diffusion-controlled, carbonation stage. Moreover, scanning electron microscopy analysis of samples after prolonged carbonation showed that pore filling occurred at the sorbent particle surfaces preventing diffusion of CO 2 toward the particle interior.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.001
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow), Research integrity
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.004
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.001
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.001
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0010.003
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.035
GPT teacher head0.304
Teacher spread0.270 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it