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Record W2078284906 · doi:10.2118/141217-ms

Treatment of Mercaptans in Canadian Condensate

2011· article· en· W2078284906 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

aboutThe title or abstract carries a Canadian signal from the geographic lexicon.
no affNo Canadian affiliation: this work is invisible to an affiliation-only frame.
No Canadian affiliation. An affiliation-only frame, the usual design, would never have seen this work. It is one of the works that make the case for inverting the frame.

Bibliographic record

VenueSPE International Symposium on Oilfield Chemistry · 2011
Typearticle
Languageen
FieldChemical Engineering
TopicOdor and Emission Control Technologies
Canadian institutionsnot available
Fundersnot available
KeywordsOdorAcroleinChemistryDimethyl sulfideDimethyl disulfideSulfurDiluentSulfideScavengerOrganic chemistryWaste managementRadicalCatalysis

Abstract

fetched live from OpenAlex

Abstract Mercaptans occur naturally in sour crude and condensate and cause an unpleasant odor which is a nuisance to operators and surrounding communities. Regulatory authorities often require control of mercaptan odors. A facility in Alberta stores condensate for use as a bitumen diluent. The condensate, which is stored in a large 110,000 barrel (bbl) (17,500 m3) holding tank, typically contains 150 to 400 ppm of total mercaptans (as sulfur). The odor resulting from these mercaptans can be detected off-site and is a nuisance to neighboring facilities. Acrolein was selected as a sulfide scavenger to reduce the mercaptan level in the condensate. At the time of treatment, the condensate had a total mercaptan level of 224 ppm. Impellers in the tank were started to mix the condensate, and then 9,260 liters of acrolein were injected into the bottom of the tank while mixing. This amount of acrolein was calculated to achieve a 50% reduction in total mercaptan content. The total mercaptan level in the condensate was actually reduced by 59%, from 224 ppm to 91 ppm (133 ppm scavenged). Acrolein scavenges all mercaptans, but preferentially reacts with the lighter mercaptans first. Ethyl and propyl mercaptan were reduced 88% and 53%, respectively. These light mercaptans were the most volatile and worst smelling mercaptans present, so their selective removal made the treatment efficient for odor reduction. Mercaptan odor was not detected at the site during the application even though the tanks were being stirred. After the application, mercaptan odors were significantly reduced and not detectable off-site. The condensate was not adversely impacted by the treatment and was able to be transported by pipeline for use in processing bitumen. This application demonstrates that condensate containing problematic levels of mercaptans can be successfully treated using acrolein, and subsequently be safely transported and used as a bitumen diluent.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesInsufficient payload (model declined to judge)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.475
Threshold uncertainty score0.999

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0020.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.019
GPT teacher head0.237
Teacher spread0.218 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it