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Record W2122079174 · doi:10.3749/canmin.47.5.1001

IMAGING ELEMENT-DISTRIBUTION PATTERNS IN MINERALS BY LASER ABLATION - INDUCTIVELY COUPLED PLASMA - MASS SPECTROMETRY (LA-ICP-MS)

2009· article· en· W2122079174 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.
fundA Canadian funder is recorded on the work.
venuePublished in a venue whose home country is Canada.

Bibliographic record

VenueThe Canadian Mineralogist · 2009
Typearticle
Languageen
FieldEngineering
TopicLaser-induced spectroscopy and plasma
Canadian institutionsLaurentian University
FundersCanada Research Chairs
KeywordsInductively coupled plasma mass spectrometryLaser ablationMass spectrometryMass spectrometry imagingAnalytical Chemistry (journal)ChemistryLaserOpticsChromatographyPhysics

Abstract

fetched live from OpenAlex

We demonstrate the application potential of laser-ablation - inductively coupled plasma - mass spectrometry (LA-ICP-MS) to map the distribution of major and trace elements in a variety of samples. The examples cover a wide range of elements, including the rare-earth elements (REE) and platinum-group elements (PGE). In order to test the capabilities of the technique, samples of different matrices were analyzed (i.e., carbonates, silicates and sulfides). The main obstacle to rapid processing of element-distribution maps by laser ablation was data processing. This has been overcome with the development of new software, such as IOLITE, and improved designs of the laser-ablation cells and refinements of commercially available laser systems. It is possible to obtain fully quantified concentration maps for single-matrix samples using parallel adjoining line-scans. Single spot-analyses will result in better precision and accuracy, but the geochemical images are superior to conventional laser-ablation spot-analysis because they reveal geochemical details that are not visible under the microscope and cannot be appreciated with single spot-analyses. In addition to providing spatial information, the individual line-scans that are used in the image acquisition offer the option to obtain quantitative results along any part of the scan. Using LA-ICP-MS imaging, our dataset reveals zoned REE distribution in garnet crystals, a heterogeneous occurrence of the PGE in sulfides, as well as the internal chemical structures in ooids with respect to conditions of growth.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: none
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.580
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.008
GPT teacher head0.216
Teacher spread0.207 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it