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Record W2317322469 · doi:10.1107/s0108767310098983

A whole new family of perovskite-based structures

2010· article· en· W2317322469 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.

Bibliographic record

VenueActa Crystallographica Section A Foundations of Crystallography · 2010
Typearticle
Languageen
FieldEngineering
TopicMicrowave Dielectric Ceramics Synthesis
Canadian institutionsNational Research Council CanadaGeological Survey of Canada
Fundersnot available
KeywordsPerovskite (structure)Materials scienceCrystallographyChemistry

Abstract

fetched live from OpenAlex

The complex and often non-linear structural response of framework structures to changes in pressure, temperature, and especially composition (e.g. the plateau effect), is due to the delicate balance of forces between the framework components of strongly-bonded polyhedra and the interactions between the framework and extra-framework species. For example, we have previously shown [1] that whether the tilts of the octahedra in perovskites increase or decrease with increasing pressure depends on the relative strength of the bonding between the framework and the extra-framework cation compared to the strength of the cation-oxygen bonds within the octahedra. Feldspars are far more structurally complex than perovskites and have previously resisted the challenge of quantifying their behaviour in this way. However, Megaw (1974) showed [2] that the rigid-unit deformations of the tetrahedral framework of feldspars can be decomposed in to four tilts of the four tetrahedra that comprise the 4-rings that lie parallel to (010). Of these four tilts Megaw showed that only two, an outward tilt of the T2 tetrahedra and a wrinkle of the 4-ring, change significantly between different alkali feldspars. Analysis of the high-pressure and high-temperature data now available, from both experiment and DFT calculations, confirms that these are the dominant tilt mechanisms. In particular, we have found that changes in the wrinkle tilt are responsible for changes in the length of the feldspar crankshaft, and are thus responsible for 70% of the volume change of alkali feldspars with P, T, or composition.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: none
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.924
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0010.001
Bibliometrics0.0020.003
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0010.000
Research integrity0.0000.001
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.007
GPT teacher head0.212
Teacher spread0.204 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it