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Record W2623930691 · doi:10.1073/pnas.1701386114

Manipulating the ABCs of self-assembly via low-χ block polymer design

2017· article· en· W2623930691 on OpenAlexaff
Alice B. Chang, Christopher M. Bates, Byeongdu Lee, C. M. Garland, Simon C. Jones, Russell K. W. Spencer, M. W. Matsen, Robert H. Grubbs

Bibliographic record

VenueProceedings of the National Academy of Sciences · 2017
Typearticle
Languageen
FieldMaterials Science
TopicBlock Copolymer Self-Assembly
Canadian institutionsUniversity of Waterloo
FundersCamille and Henry Dreyfus FoundationArgonne National LaboratoryU.S. Department of DefenseNational Science Foundation
KeywordsLamellar structurePolymerConverseCopolymerMaterials scienceChemical physicsTransmission electron microscopyDomain (mathematical analysis)Block (permutation group theory)Morphology (biology)Self-assemblySoft matterMolar massLamellar phaseCrystallographyNanotechnologyPhysicsChemistryMathematicsColloidComposite material

Abstract

fetched live from OpenAlex

Significance Molecular sequence and interactions dictate the mesoscale structure of all self-assembling soft materials. Block polymers harness this relationship to access a rich variety of nanostructured materials but typically require energetically unfavorable (high-χ) interactions between blocks. Contrary to this convention, we demonstrate that ABC triblock terpolymers featuring low-χ interactions between end blocks can self-assemble into a unique mixed morphology that subverts the demands of chain connectivity. As a consequence of block–block mixing, the characteristic length scales of these self-assembled structures exhibit an unusual trend: As the total polymer size increases, the domain spacing decreases. These developments expand the vocabulary of block polymer design and open additional avenues for manipulating the self-assembly of synthetic macromolecules.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.001
Threshold uncertainty score0.004

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.046
GPT teacher head0.301
Teacher spread0.255 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations60
Published2017
Admission routes1
Has abstractyes

Explore more

Same venueProceedings of the National Academy of SciencesSame topicBlock Copolymer Self-AssemblyFrench-language works237,207