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Harmonizing lipidomics: NIST interlaboratory comparison exercise for lipidomics using SRM 1950–Metabolites in Frozen Human Plasma

2017· article· en· 411 citations· W2764166773 on OpenAlex· 10.1194/jlr.m079012

Why is this work in the frame?

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

Canadian affiliationAn author listed a Canadian institution. This is the only route the usual frame has.
Canadian funderA Canadian agency funded it. The work may carry no Canadian affiliation at all.

Full frame distilled prediction

Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

Candidate categories
none
Consensus categories
none
Domain
Candidate signal: noneConsensus signal: none
Study design
Candidate signal: Bench or experimentalConsensus signal: Bench or experimental
Genre
Candidate signal: EmpiricalConsensus signal: Empirical
Teacher disagreement score
0.166
Threshold uncertainty score
0.874
Validation status
machine_predicted_unvalidated · codex-gemma-dda1882f352a

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0040.001
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0010.000
Bibliometrics0.0010.000
Science and technology studies0.0010.000
Scholarly communication0.0000.000
Open science0.0010.001
Research integrity0.0000.001
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Opus teacher head0.201
GPT teacher head0.445
Teacher spread
0.244 · how far apart the two teachers sit on this one work
Validation status
score_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Abstract

As the lipidomics field continues to advance, self-evaluation within the community is critical. Here, we performed an interlaboratory comparison exercise for lipidomics using Standard Reference Material (SRM) 1950-Metabolites in Frozen Human Plasma, a commercially available reference material. The interlaboratory study comprised 31 diverse laboratories, with each laboratory using a different lipidomics workflow. A total of 1,527 unique lipids were measured across all laboratories and consensus location estimates and associated uncertainties were determined for 339 of these lipids measured at the sum composition level by five or more participating laboratories. These evaluated lipids detected in SRM 1950 serve as community-wide benchmarks for intra- and interlaboratory quality control and method validation. These analyses were performed using nonstandardized laboratory-independent workflows. The consensus locations were also compared with a previous examination of SRM 1950 by the LIPID MAPS consortium. While the central theme of the interlaboratory study was to provide values to help harmonize lipids, lipid mediators, and precursor measurements across the community, it was also initiated to stimulate a discussion regarding areas in need of improvement.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

The record

Venue
Journal of Lipid Research
Topic
Metabolomics and Mass Spectrometry Studies
Field
Biochemistry, Genetics and Molecular Biology
Canadian institutions
Concordia UniversityUniversity of VictoriaMcGill UniversityHospital for Sick ChildrenGenome British ColumbiaJewish General Hospital
Funders
Advanced Low Carbon Technology Research and Development ProgramCore Research for Evolutional Science and TechnologyNational Center for Advancing Translational SciencesOffice of Experimental Program to Stimulate Competitive ResearchNational Center for Research ResourcesNational Institute of Diabetes and Digestive and Kidney DiseasesNational Heart, Lung, and Blood InstituteNatural Sciences and Engineering Research Council of CanadaCanadian Institutes of Health ResearchNational Institute of Standards and TechnologyNational Research Foundation SingaporeNational Institute for Health Research Southampton Biomedical Research CentreDirectorate for Biological SciencesNational Institutes of HealthNational Institute of General Medical SciencesWarren Y. Soper Charitable TrustNational Cancer InstituteGenome AlbertaJapan Science and Technology AgencyGeorgia Clinical and Translational Science AllianceVetenskapsrådetHjärt-LungfondenAustrian Science FundNational University of SingaporeNational Research FoundationLeading Edge Endowment FundMcGill UniversityJapan Agency for Medical Research and DevelopmentGenome British ColumbiaFondation De Famille Alvin SegalSteno Diabetes Center CopenhagenKansas IDeA Network of Biomedical Research ExcellenceJewish General HospitalNational Institute for Health and Care ResearchGenome CanadaNational Science Foundation
Keywords
LipidomicsNISTWorkflowChemistryComputer scienceBiochemistryDatabase
Has abstract in OpenAlex
yes