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Design of N-Coordinated Dual-Metal Sites: A Stable and Active Pt-Free Catalyst for Acidic Oxygen Reduction Reaction

2017· article· en· 1,585 citations· W2768340505 on OpenAlex· 10.1021/jacs.7b10385

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Abstract

We develop a host-guest strategy to construct an electrocatalyst with Fe-Co dual sites embedded on N-doped porous carbon and demonstrate its activity for oxygen reduction reaction in acidic electrolyte. Our catalyst exhibits superior oxygen reduction reaction performance, with comparable onset potential ( E onset, 1.06 vs 1.03 V) and half-wave potential ( E 1/2, 0.863 vs 0.858 V) than commercial Pt/C. The fuel cell test reveals (Fe,Co)/N-C outperforms most reported Pt-free catalysts in H 2 /O 2 and H 2 /air. In addition, this cathode catalyst with dual metal sites is stable in a long-term operation with 50 000 cycles for electrode measurement and 100 h for H 2 /air single cell operation. Density functional theory calculations reveal the dual sites is favored for activation of O-O, crucial for four-electron oxygen reduction.

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The record

Venue
Journal of the American Chemical Society
Topic
Electrocatalysts for Energy Conversion
Field
Energy
Canadian institutions
Queen's University
Funders
National Key Research and Development Program of ChinaNational Synchrotron Radiation LaboratoryNational Supercomputing Center, Korea Institute of Science and Technology InformationMinistry of Science and Technology of the People's Republic of ChinaNational Natural Science Foundation of China
Keywords
ChemistryCatalysisElectrocatalystOxygenElectrolyteOxygen reduction reactionInorganic chemistryMetalCathodeElectrochemistryElectrodePhysical chemistryOrganic chemistry
Has abstract in OpenAlex
yes