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Record W4310177365 · doi:10.21203/rs.3.rs-2241549/v1

Modelling of the effect of ATH fillers on the rheology, curing kinetics, and flexural properties of the epoxy resin forming the hydraulic turbines' stay vanes extension

2022· preprint· en· W4310177365 on OpenAlexafffund
Rim Ouadday, Rachid Boukhili, Aurélian Vadean, Mahmoud Abusrea

Bibliographic record

VenueResearch Square · 2022
Typepreprint
Languageen
FieldEngineering
TopicEpoxy Resin Curing Processes
Canadian institutionsPolytechnique Montréal
FundersNatural Sciences and Engineering Research Council of Canada
KeywordsMaterials scienceEpoxyComposite materialCuring (chemistry)Flexural strengthRheologyFlexural modulusPolymerizationShrinkagePolymer

Abstract

fetched live from OpenAlex

Abstract Epoxy resins are essential for the manufacturing of GFRP/XPS foam sandwich structures used for hydraulic turbine extension stay vanes. Their properties during and after curing are key factors for the performance of the entire hybrid composite structure. This paper introduces experimental characterization and modeling of the influence of the quantity and size of ATH fillers on the curing and post-curing characteristics of the epoxy resin. The experimental investigation involves the maximum temperature, polymerization time, shrinkage, viscosity, and flexural properties. The mass fractions of the ATH were 10, 20, 30, 40, 50, and 60%, and the particle sizes were 2, 4, 6, 8, and 12 µm. In addition, we utilized the multivariate polynomial regression (MPR) and artificial neural network (ANN) methods to develop empirical models to predict the maximum temperature, polymerization time, shrinkage, and flexural modulus. The experimental results showed that increasing ATH mass fraction with smaller particle size delayed polymerization and lowered the maximum temperature. The experimental viscosity values showed that Mooney model can accurately calculate viscosity as a function of ATH mass fraction and particle size, compared to the Quemada and Krieger-Dougherty models. Adding ATH increased flexural strength, modulus, and breakage strain. The developed models achieved a higher than 0.9 correlation coefficient between the predicted and measured responses and can be used to enhance the design and control the casting of the proposed sandwich structures.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: none
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.003
Threshold uncertainty score0.006

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.001
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0010.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.070
GPT teacher head0.303
Teacher spread0.232 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations1
Published2022
Admission routes2
Has abstractyes

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