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Record W4388139675 · doi:10.1002/agt2.452

Spontaneous hierarchical surface engineering of minerals through coupled dissolution‐precipitation chemistry

2023· article· en· W4388139675 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.
fundA Canadian funder is recorded on the work.

Bibliographic record

VenueAggregate · 2023
Typearticle
Languageen
FieldMaterials Science
TopicCalcium Carbonate Crystallization and Inhibition
Canadian institutionsUniversity of Alberta
FundersNational Key Research and Development Program of ChinaNatural Sciences and Engineering Research Council of CanadaNatural Science Foundation of Jiangsu ProvinceNational Natural Science Foundation of China
KeywordsDissolutionCalciteMicrostructurePrecipitationAragoniteBiomineralizationMaterials scienceNanotechnologyChemical engineeringMineralogyChemistryComposite material

Abstract

fetched live from OpenAlex

Abstract Peculiar hierarchical microstructures in creatures inspire modern material design with distinct functionalities. Creatures can effortlessly construct sophisticated yet long‐range ordered microstructure across bio‐membrane through ion secretion and precipitation. However, microstructure biomimicry in current technology generally requires elaborate, point‐by‐point fabrication. Herein, a spontaneous yet controllable strategy is developed to achieve surface microstructure engineering through a natural surface phenomenon similar to ion secretion‐precipitation, that is, coupled dissolution‐precipitation. A series of hierarchical microstructures on mineral surfaces in fluids with tunable morphology, orientation, dimension, and spatial distribution are achieved by simply controlling initial dissolution and fluid chemistry. In seawater, long‐range ordered film of vertically aligned brucite flakes forms through interfacial dissolution, nucleation, and confinement‐induced orientation of flakes with vertically grown {110} plane, on the edge of which, fusiform aragonite epitaxially precipitates. With negligible initial surface dissolution, prismatic aragonite epitaxially grows on a calcite polyhedron‐packed surface. By tuning fluid chemistry, closely packed calcite polyhedron and loosely packed calcite micro‐pillars are engineered through rapid and retarded precipitation, respectively. Surprisingly, the spontaneously grown microstructures resemble those deliberately created by human or found in nature, and tremendously modulate surface functionality. These findings open new possibilities for facile and customizable engineering of microstructural surfaces, hierarchical heterostructures, and biomimetic materials.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.087
Threshold uncertainty score0.462

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.014
GPT teacher head0.242
Teacher spread0.228 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it