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Record W4395670457 · doi:10.1002/pc.28473

Chemo‐rheological and quantitative dispersion analysis of <scp>mass‐produced graphene‐unsaturated</scp> polyester based nanocomposites

2024· article· en· W4395670457 on OpenAlexafffund
Farnaz Mazaheri Karvandian, David‐Michael Phillips, Emi Myzeqari, Pascal Hubert

Bibliographic record

VenuePolymer Composites · 2024
Typearticle
Languageen
FieldEngineering
TopicEpoxy Resin Curing Processes
Canadian institutionsMcGill UniversityAS Composite (Canada)
FundersNatural Sciences and Engineering Research Council of Canada
KeywordsGrapheneMaterials scienceNanocompositeCuring (chemistry)RheologyComposite materialPolyesterDispersion (optics)Dispersion stabilityPolymerNanotechnology

Abstract

fetched live from OpenAlex

Abstract Recent advancements in mass production of graphene powders utilize less energy‐intensive methods and milder chemicals compared to traditional lab‐scale techniques. This can influence the properties of the resulting graphene particles. This study investigates the effect of mass‐produced graphene powder on the curing and rheological properties of a resin transfer molding (RTM) grade unsaturated polyester resin. An objective dispersion quantification method was established to track the dispersion state of the nanocomposite throughout the curing process. The findings reveal that the graphene powder accelerated the curing evidenced by a shift in the peak temperature and gel point towards lower values. The sample containing 1 wt.% graphene exhibited remarkable dispersion stability with only 7.1% decrease by gelation. The resin matrix's low viscosity enhanced graphene particles mobility, while its fast‐curing nature allowed less time for agglomeration. Highlights Characterization of unsaturated polyester nanocomposites modified with an industrial‐grade graphene powder Real‐time in‐situ monitoring of graphene's dispersion state Quantification dispersion analysis for an objective dispersion assessment

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.001
Threshold uncertainty score0.003

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.013
GPT teacher head0.242
Teacher spread0.229 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations8
Published2024
Admission routes2
Has abstractyes

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