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Record W4405363780 · doi:10.1016/j.dche.2024.100207

Ensemble machine learning to accelerate industrial decarbonization: Prediction of Hansen solubility parameters for streamlined chemical solvent selection

2024· article· en· W4405363780 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.
fundA Canadian funder is recorded on the work.

Bibliographic record

VenueDigital Chemical Engineering · 2024
Typearticle
Languageen
FieldMaterials Science
TopicCrystallization and Solubility Studies
Canadian institutionsPolytechnique MontréalNatural Resources Canada
FundersCanadian Forest ServiceOffice of Energy Research and DevelopmentNatural Sciences and Engineering Research Council of Canada
KeywordsSolubilitySelection (genetic algorithm)SolventComputer scienceHildebrand solubility parameterMachine learningProcess (computing)ChemistryProcess engineeringBiochemical engineeringArtificial intelligenceThermodynamicsEngineeringOrganic chemistryPhysics

Abstract

fetched live from OpenAlex

Several processes and strategies have been developed to promote the utilization of lignin and to facilitate its market adoption across a broad spectrum of applications within the expanding lignin bioeconomy. However, the inherent variability in lignin properties, resulting from diverse feedstock sources and varied recovery and downstream processing methods, remains a significant challenge. This highlights the critical need to investigate lignin's miscibility and reactivity with polymers and solvents, as most lignin valorization pathways involve mixing, blending, or solubilization. Accurate estimation of Hansen solubility parameters (HSP) is crucial for solvent selection in several fields such as polymer science, coatings, adhesives, lignin-based biorefineries and solvent-based carbon capture. Traditional methods for predicting HSP are time-consuming and involve complex experiments, especially in applications dealing with carbon dioxide and lignin solubility. This paper introduces a novel ensemble modeling methodology based on machine learning (ML) techniques for accurate HSP prediction using Simplified Molecular Input Line Entry System (SMILES) codes as entries. The methodology integrates different ML approaches, including deep and shallow learning, to enhance prediction accuracy. Decision fusion of individual ML models is achieved through a hybrid approach combining non-learnable and learnable methods, resulting in reduced errors and enhanced accuracy. The results highlight the effectiveness of the ensemble-based methodology, which achieved 99% accuracy in predicting dispersion solubility parameters, outperforming other individual ML techniques. The proposed generic methodology, from data preprocessing to decision fusion through diverse ML algorithms, can be applied to various chemical analytics beyond HSP prediction.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.001
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.247
Threshold uncertainty score0.647

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.001
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.032
GPT teacher head0.241
Teacher spread0.209 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it