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Record W4406030421 · doi:10.1088/2053-1591/ada5c4

Effect of pretreatment type on the physico-chemical properties of activated carbons derived from an invasive weed Prosopis juliflora: potential applications

2025· article· en· W4406030421 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.
fundA Canadian funder is recorded on the work.

Bibliographic record

VenueMaterials Research Express · 2025
Typearticle
Languageen
FieldChemistry
TopicAdsorption, diffusion, and thermodynamic properties of materials
Canadian institutionsMemorial University of Newfoundland
FundersDepartment of Science and Technology, Ministry of Science and Technology, IndiaMitacsAuburn University
KeywordsProsopis julifloraWeedActivated carbonChemistryBiologyAgronomyOrganic chemistryAdsorption

Abstract

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Abstract This study investigates the effects of various pretreatment methods on the physico-chemical properties of activated carbons produced from the biochar of an invasive weed species, Prosopis juliflora . Utilizing a thermochemical conversion technique such as pyrolysis, followed by chemical and physical activation processes, we aimed to assess the functional characteristics of the resulting biochar for potential industrial applications. The pretreatments involved acidic (H 2 SO 4 , H 3 PO 4 , and ZnCl 2 ), basic (KOH and NH 4 OH) and oxidizing agents (H 2 O 2 ), and physical methods like air activation. Comprehensive characterization techniques, namely BET analysis, x-ray Photoelectron Spectroscopy (XPS), Ultimate Analysis, and pH pzc , were utilized to assess the influence of activation conditions. Principal component analysis was employed to elucidate the relationships between different activation methods and the physico-chemical properties of the activated carbons. Results from this study revealed that the choice of activation agent significantly influences the material’s structure and chemistry. The activation process of activated carbon (AC) is significantly influenced by temperature and the agent used. KOH-AC exhibited bulk oxygen content (5.96%) with a high bulk carbon content (91.73%), while Air-AC has a comparatively high bulk oxygen content (40.71%). The XPS data shows variations in carbon content and oxygen functional groups, influenced by the activation agent and temperature used during the process. The ranking of surface oxygen content was Air-AC (39.93%) > H 2 O 2 -AC (22.77%) > NH 4 OH-AC (17.61%). This study highlights the potential of Prosopis juliflora -derived biochar in diverse applications by tailoring its physico-chemical properties through specific activation processes, thereby also contributing to the upcycling of this invasive species.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.004
Threshold uncertainty score0.596

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0010.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.026
GPT teacher head0.301
Teacher spread0.275 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it