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Automated Predictive Chemical Reaction Modelling applied to Gold(I) Catalysis

2025· preprint· en· W4408464062 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.
fundA Canadian funder is recorded on the work.

Bibliographic record

VenueChemRxiv · 2025
Typepreprint
Languageen
FieldMaterials Science
TopicMachine Learning in Materials Science
Canadian institutionsUniversité de Sherbrooke
FundersHydro-Québec
KeywordsCatalysisComputer scienceChemistryBiochemical engineeringEngineeringOrganic chemistry

Abstract

fetched live from OpenAlex

Computational modelling is a powerful tool to study chemical reactions. Currently, human guidance is nearly always required to avoid the untractable complexity of all a priori possible reaction steps, which consequently greatly limits automated predictive applications. Despite recent advances in the field, predictive reaction modelling without human guidance remains limited. In this work, we present a theoretical framework based on atomic reactivity as well as a "neophile" kinetic model, demonstrating how they enable unbiased automated reaction modelling with molecules of size typically encountered in experimental methodologies. Our framework allows the identification of unlikely or redundant reaction steps based on first principles and previous analyses, while the neophile kinetic model separates crucial reaction intermediates from inconsequential ones. These advances greatly improved modelling efficiency and allowed us to automatically model 17 unimolecular gold(I)-catalyzed reactions of increasing complexity starting only from the reactant and catalyst. In 11 reactions, the experimental product distribution is closely reproduced, with an additional 4 being essentially correct. Our results demonstrate that it is possible to predictively model catalytic reactions without human guidance through a convenient reformulation of the problem. We anticipate that this work will enable the rapid generation of unbiased reaction data. In addition to providing chemical insight, this data could train machine-learning models to manifest mechanism-based chemical reasoning. These models could eventually be combined with self-driving laboratories to form powerful self-teaching, self-correcting autonomous research agents.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.042
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.000
Meta-epidemiology (narrow)0.0010.001
Meta-epidemiology (broad)0.0010.000
Bibliometrics0.0000.001
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0010.002
Research integrity0.0010.001
Insufficient payload (model declined to judge)0.0000.001

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.016
GPT teacher head0.272
Teacher spread0.256 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it