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Record W4412523034 · doi:10.1016/j.jmr.2025.107923

Rapid flow characterization measurements using a modified CPMG measurement with incremented echo times, phase cycling and filtering

2025· article· en· W4412523034 on OpenAlexafffund
Sebastian Richard, Benedict Newling, Bruce J. Balcom

Bibliographic record

VenueJournal of Magnetic Resonance · 2025
Typearticle
Languageen
FieldEngineering
TopicFlow Measurement and Analysis
Canadian institutionsUniversity of New Brunswick
FundersNatural Sciences and Engineering Research Council of Canada
KeywordsEcho (communications protocol)Characterization (materials science)Phase (matter)Nuclear magnetic resonanceCyclingAnalytical Chemistry (journal)Flow (mathematics)ChemistryMaterials sciencePhysicsNanotechnologyChromatographyComputer scienceMechanics

Abstract

fetched live from OpenAlex

We recently demonstrated a magnetic resonance methodology for measuring and characterizing various pipe flows, using a series of individually-acquired spin echoes at different τ . The key advantage of our approach lies in the simplicity of the experiment, MR hardware, and data processing. However, acquiring each spin echo separately results in prolonged measurement times. To address this, we employ an echo-train approach to acquire the series of variable τ spin echoes. By incrementing CPMG echo pulse spacings within the echo train and implementing a four-step phase cycling scheme to suppress coherence pathway effects, we obtain the same echo phase and magnitude response to flow as a function of τ 2 as in our original method, without requiring individual echo acquisitions. This new approach significantly reduces the number of required experiments, shortening measurement time by a factor of 1 / N , where N is the number of utilized echoes per echo train. Our phase cycling strategy, combined with incremented pulse spacings, enables N = 3 in our benchtop flow measurement. Validation experiments with Newtonian and shear-thinning fluids confirm that the new echo-train technique yields results consistent with the original approach of acquiring each spin echo separately. • A CPMG echo train in the presence of magnetic field gradient encodes velocity. • Variable τ along the train imparts different flow sensitivity to different echoes. • Phase-cycling and filtering select for the direct echo. • Data are fit with an analytical model of the magnetic resonance signal. • Apparatus is low-field and portable for magnetic resonance rheometry.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.002
metaresearch head score (Gemma)0.001
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: none
Teacher disagreement score0.002
Threshold uncertainty score0.010

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0020.001
Meta-epidemiology (narrow)0.0010.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0010.001
Science and technology studies0.0000.001
Scholarly communication0.0000.001
Open science0.0010.001
Research integrity0.0010.001
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.035
GPT teacher head0.236
Teacher spread0.201 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations0
Published2025
Admission routes2
Has abstractyes

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