Theoretical and Experimental Analysis of Miniaturization of Conventional Oscillatory Flow Technology
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Résumé
The requirement for any configuration of a chemical or biochemical reactor is the presence of efficient mixing to enhance heat and mass transfer as needed for the application of interest. Furthermore, as an Oscillatory Flow (OF) reactor has a combination of flow oscillation and baffled tube configuration, which has the potential to ensure efficient mixing, heat transfer, and mass transfer. In this way, an efficient mixing in an OF reactor is able to tackle any type of resistance in any chemical process from polymer synthesis to enzyme production. It has been observed that an OF reactor improved both conversion and selectivity of the relevant reaction by efficient mixing and transport properties. However, this technology was not still extended to mini-fluidic configuration via process intensification methods and so far, a novel approach for enhanced mixing at reduced scales was not explored. This work explores the application of OF technology in mini-fluidics. The feasibility analysis of Oscillatory Flow Technology in mini channels has been investigated using theoretical correlations from Conventional Oscillatory flow technology in process equipment. As a preliminary step in the process intensification of OF technology in mini channels, The Nusselt number (Nu) and pressure drop values are predicted from the literature and it has been observed that the transfer operations are also improved when oscillatory flow is applied in mini channels compared to commercial mini contactors such as corning heart shaped reactor. The plot between energy dissipation vs. mixing evaluated from theoretical calculations was drawn and compared with mini-fluidic mixers reported in literature. The most common mini-fluidic mixer is corning heart shaped reactor used for comparison with the proposed minichannel. Because of this analysis, the novel mixing geometries was expected to develop for various chemical processing applications. The OFT experimental set up was developed to create oscillatory flow via either forward rotation or backward rotation of valve. Furthermore, pressure vs. time profile and flow vs. time profile for the given OF mini fluidic arrangement is initially investigated and described. Preliminary experimental results are provided for an OF generator, intended for use in subsequent experiments exploring mini-fluidic mixers with OF technology.
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Scores Codex et Gemma par catégorie
| Catégorie | Codex | Gemma |
|---|---|---|
| Métarecherche | 0,002 | 0,000 |
| Méta-épidémiologie (sens strict) | 0,000 | 0,000 |
| Méta-épidémiologie (sens large) | 0,000 | 0,000 |
| Bibliométrie | 0,002 | 0,004 |
| Études des sciences et des technologies | 0,000 | 0,001 |
| Communication savante | 0,000 | 0,000 |
| Science ouverte | 0,001 | 0,000 |
| Intégrité de la recherche | 0,000 | 0,000 |
| Charge utile insuffisante (le modèle a refusé de juger) | 0,000 | 0,000 |
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