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Record W1967539549 · doi:10.1017/s0885715613000638

Unit-cell parameters for scapolite solid solutions and a discontinuity at <i>Me</i> <sub>75</sub> , ideally NaCa <sub>3</sub> [Al <sub>5</sub> Si <sub>7</sub> O <sub>24</sub> ](CO <sub>3</sub> )

2013· article· en· W1967539549 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.

Bibliographic record

VenuePowder Diffraction · 2013
Typearticle
Languageen
FieldMaterials Science
TopicX-ray Diffraction in Crystallography
Canadian institutionsUniversity of Calgary
Fundersnot available
KeywordsEMPACrystallographyDiscontinuity (linguistics)Electron microprobeSolid solutionRietveld refinementFormula unitMaterials scienceCrystal structureAnalytical Chemistry (journal)ChemistryMineralogyMathematicsMathematical analysisMetallurgy

Abstract

fetched live from OpenAlex

Twenty-seven scapolite samples from various localities and with compositions between Me 6–93 were obtained using electron microprobe analysis (EMPA). Their unit-cell parameters were obtained using synchrotron high-resolution powder X-ray diffraction (HRPXRD) data and Rietveld structure refinements using space group P 4 2 / n . The EMPA data show the well-known discontinuity at Me 75 . In addition, the unit-cell parameters, especially c , show a discontinuity at Me 75 (=five Al atoms per formula unit, apfu ), ideally NaCa 3 [Al 5 Si 7 O 24 ](CO 3 ), where the scapolite solid solution is divided into two ( Me % = [Ca/(Ca + Na + K)] × 100). A maximum c parameter value occurs at Me 37.5 (=four Al apfu ideally), where complete Al–Si, Na–Ca, and Cl–CO 3 order occurs. The unit-cell volume, V , varies smoothly with Me % and Al apfu across the series.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.004
metaresearch head score (Gemma)0.002
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow), Science and technology studies, Scholarly communication, Research integrity, Insufficient payload (model declined to judge)
Consensus categoriesMeta-epidemiology (narrow), Science and technology studies, Research integrity
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.025
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0040.002
Meta-epidemiology (narrow)0.0040.005
Meta-epidemiology (broad)0.0040.003
Bibliometrics0.0030.003
Science and technology studies0.0050.003
Scholarly communication0.0030.009
Open science0.0020.002
Research integrity0.0030.004
Insufficient payload (model declined to judge)0.0000.003

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.019
GPT teacher head0.249
Teacher spread0.230 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it