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Mechanical and Rheological Properties of Polyurethane Elastomers from Hydroxy-Terminated Polybutadiene and Isophorone Diisocyanate Used as Liners for Composite Propellants

2015· article· en· W1970890503 on OpenAlex
Javier Quagliano, Víctor Wittemberg, Jorge Luis González-Velázquez, Alejandro Bacigalupe

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

venuePublished in a venue whose home country is Canada.
no affNo Canadian affiliation: this work is invisible to an affiliation-only frame.
No Canadian affiliation. An affiliation-only frame, the usual design, would never have seen this work. It is one of the works that make the case for inverting the frame.

Bibliographic record

VenueJournal of Research Updates in Polymer Science · 2015
Typearticle
Languageen
FieldMaterials Science
TopicPolymer Nanocomposites and Properties
Canadian institutionsnot available
Fundersnot available
KeywordsIsophorone diisocyanateMaterials scienceThixotropyPolybutadieneComposite materialHydroxyl-terminated polybutadienePolyurethaneIsophoroneUltimate tensile strengthCuring (chemistry)Dynamic mechanical analysisPolymer chemistryPolymerDiamine

Abstract

fetched live from OpenAlex

In this contribution, we studied mechanical and rheological properties of liners based on hydroxy terminated polybutadiene (HTPB) loaded with titanium dioxide and cured with isophorone diisocyanate (IPDI) or toluene diisocyanate (TDI). A thixotropic agent (Thixin R) was added, and viscosity was measured as a function of curing time, leading to much lower viscosities and longer pot life values. Mechanical properties (tensile strength and elongation at break) were not significantly affected but viscosity was reduced at all tested concentrations. Loss modulus (G'') and storage modulus (G') were measured during cure time at three different temperatures (7, 25 and 60°C) with IPDI, and at 7 and 25°C for TDI. Both curves did not intersect during the cure period studied (120 minutes) for IPDI but did so for TDI at 25°C with the formulation having a thixotropic additive. These results suggested that liner formulations will flow if sprayed onto the inner surface of the rocket case before propellant is casted.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.005
metaresearch head score (Gemma)0.001
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesScience and technology studies
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.025
Threshold uncertainty score0.999

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0050.001
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0010.000
Bibliometrics0.0010.001
Science and technology studies0.0000.003
Scholarly communication0.0000.001
Open science0.0010.001
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.079
GPT teacher head0.353
Teacher spread0.273 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it