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Record W1975858595 · doi:10.1080/10426500590906238

Mimetics of the Selenoenzyme Glutathione Peroxidase: Novel Structures and Unusual Catalytic Mechanisms

2005· article· en· W1975858595 on OpenAlexaffabout
Thomas G. Back, Ziad Moussa

Bibliographic record

VenuePhosphorus, sulfur, and silicon and the related elements · 2005
Typearticle
Languageen
FieldPharmacology, Toxicology and Pharmaceutics
TopicOrganoselenium and organotellurium chemistry
Canadian institutionsUniversity of Calgary
Fundersnot available
KeywordsSelenideSeleniumChemistryPeroxidaseGlutathione peroxidaseCatalysisThiolGlutathioneCombinatorial chemistryGPX3PropargylEnzymeOrganic chemistry

Abstract

fetched live from OpenAlex

Glutathione peroxidase (GPx) mimetics comprise an important class of selenium-containing antioxidants that catalyze the destruction of biologically harmful peroxides in the presence of stoichiometric thiol reductants. The synthesis of two novel cyclic selenium compounds and their evaluation as GPx mimetics was achieved. The first is a cyclic seleninate ester that is formed in situ from the oxidation of allyl 3-hydroxypropyl selenide. The second is a spirodioxyselenurane that is similarly formed from di(3-hydroxypropyl) selenide. Both compounds were shown to be remarkably active catalysts in an assay based on the reduction of t-butyl hydroperoxide with benzyl thiol. The mechanisms of the catalytic cycles of the two novel selenium compounds were elucidated and were found to be distinct from each other and from that of GPx. Keywords: Cyclic seleninate estersglutathione peroxidase mimeticsspirodioxyselenuranes Acknowledgments We thank the Natural Sciences and Engineering Research Council of Canada for financial support.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.059
Threshold uncertainty score0.791

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.001
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.001
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.021
GPT teacher head0.305
Teacher spread0.285 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations5
Published2005
Admission routes2
Has abstractyes

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