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Record W1977929769 · doi:10.1021/jp046626j

One-Electron Oxidation of Methionine in Peptide Environments:  The Effect of Three-Electron Bonding on the Reduction Potential of the Radical Cation

2004· article· en· W1977929769 on OpenAlexafffund
Patrick Brunelle, Arvi Rauk

Bibliographic record

VenueThe Journal of Physical Chemistry A · 2004
Typearticle
Languageen
FieldChemistry
TopicFree Radicals and Antioxidants
Canadian institutionsUniversity of Calgary
FundersAlzheimer Society
KeywordsChemistryRadicalSolvationRadical ionBond-dissociation energyAmine gas treatingDissociation (chemistry)SulfideRedoxAmideAmino acidMedicinal chemistryComputational chemistryCrystallographyStereochemistryInorganic chemistryPhysical chemistryOrganic chemistryMoleculeIon

Abstract

fetched live from OpenAlex

The complexes between the radical cation of dimethyl sulfide 2 and models for eight biologically available electron pair donors,:X (:X = H 2 O ( 2a ), H 2 CO ( 2b ), HC(O)NH 2 ( 2c ), HC(O)NHCH 3 ( 2d ), HCO 2 - ( 2e ), HCO 3 - ( 2f ), H 2 PO 4 - ( 2g ), and CH 3 NH 2 ( 2h )), were optimized at the B3LYP/6-31G(d) level of theory. S∴X bond dissociation enthalpies (BDEs) were determined by single point calculations at the CBS−RAD level, a method designed for quantitative thermochemistry of free radicals. The effect of solvation was determined by application of a polarizable continuum model. Only the amine complex is predicted to be stable in water. H 2 O and H 2 PO 4 - make transient complexes, and the remaining complexes are predicted to dissociate spontaneously. The dissociation is driven by entropy and conformationally constrained complexes are predicted to be stable in water. Reduction potentials, E °, accurate to ±0.1 V were calculated for the complexes with dimethyl sulfide and for the amino acid, methionine, both as an isolated amino acid and incorporated into a polypeptide at the N- and C-terminals and midchain. Stabilization of the radical cation of Met by three-electron bonding is predicted if an S∴N bond can be formed to a free amino group, as in N-terminal Met or a nearby Lys. Likewise, Met oxidation is facilitated by phosphodiesters, but not by carboxylate groups or amide groups. No lowering of E ° is predicted for C-terminal Met or for midchain Met. The implications of the results for the redox chemistry associated with Alzheimer's disease are discussed.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.006
Threshold uncertainty score0.322

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0010.000
Research integrity0.0000.001
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.006
GPT teacher head0.228
Teacher spread0.222 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations58
Published2004
Admission routes2
Has abstractyes

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