New zircon shock phenomena and their use for dating and reconstruction of large impact structures revealed by electron nanobeam (EBSD, CL, EDS) and isotopic U–Pb and (U–Th)/He analysis of the Vredefort domeThis article is one of a series of papers published in this Special Issue on the theme of <i>Geochronology</i> in honour of Tom Krogh.
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Abstract
Integrated electron nanobeam (EBSD, CL, EDS) and isotopic measurements (U–Pb, (U–Th)/He) of zircon from the collar and centre of the 80 km wide central uplift of the 2020 ± 3 Ma Vredefort impact structure reveal new shock features in a microstructural progression related to impact basin formation and degree of U–Pb age resetting: (1) planar fractures in {1K0} and {1K2} orientation during initial shock wave compression; (2) curviplanar fractures in {1K1} orientation, now annealed, which host glassy inclusions of partial melt of the host rock; (3) microtwin lamellae in an orientation of 65° about [110], attributed to shock wave rarefaction; (4) nucleation of impact-age crystallites, possibly on microtwins, during post-shock heating by impact melt; and (5) crystal-plastic deformation linked to crater modification of the core of the central uplift. Planar fracturing and microtwinning ≥20 GPa in “cold shock” zircon in granitoid at a radial distance of 25 km failed to reset zircon age. Single-grain ID–TIMS data extend between pre-impact age of 2077 ± 11 Ma and a secondary Pb-loss event at ca. 1.0 Ga — the latter reflecting Kibaran igneous activity between 1.110 and 1.021 Ga. Age resetting by the impact event operated in an ∼15 km wide “hot shock” zone of impact-elevated temperatures ≥700 °C at the core of the central uplift. Mechanisms include internal recrystallization, defect-accelerated Pb diffusion via shock microstructures and melt films, and late crystal-plastic deformation. Igneous zircons from a 2019 ± 2 Ma foliated norite impact melt yield a mean (U–Th)/He date of 923 ± 61 Ma, indicating exposure of the present surface after this time.
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Teacher imitationNot calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.
Codex and Gemma teacher scores by category
| Category | Codex | Gemma |
|---|---|---|
| Metaresearch | 0.001 | 0.000 |
| Meta-epidemiology (narrow) | 0.000 | 0.000 |
| Meta-epidemiology (broad) | 0.000 | 0.000 |
| Bibliometrics | 0.000 | 0.001 |
| Science and technology studies | 0.000 | 0.001 |
| Scholarly communication | 0.000 | 0.000 |
| Open science | 0.000 | 0.000 |
| Research integrity | 0.000 | 0.000 |
| Insufficient payload (model declined to judge) | 0.002 | 0.000 |
Machine scores (provisional)
The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.
Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.
score_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it