Shape-Controlled Synthesis of Highly Crystalline Titania Nanocrystals
Why this work is in the frame
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Bibliographic record
Abstract
A versatile synthetic method based on solvothermal technique has been developed for the fabrication of TiO(2) nanocrystals with different shapes such as rhombic, truncated rhombic, spherical, dog-bone, truncated and elongated rhombic, and bar. The central features of our approach are the use of water vapor as hydrolysis agent to accelerate the reaction and the use of both oleic acid and oleylamine as two distinct capping surfactants which have different binding strengths to control the growth of the TiO(2) nanoparticles. We also show that the presence of an appropriate amount of water vapor along with the desired oleic acid/oleylamine molar ratio plays a crucial role in controlling size and shape of TiO(2) nanocrystals.
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Full frame distilled prediction
Teacher imitationNot calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.
Codex and Gemma teacher scores by category
| Category | Codex | Gemma |
|---|---|---|
| Metaresearch | 0.000 | 0.000 |
| Meta-epidemiology (narrow) | 0.000 | 0.000 |
| Meta-epidemiology (broad) | 0.001 | 0.000 |
| Bibliometrics | 0.000 | 0.000 |
| Science and technology studies | 0.000 | 0.000 |
| Scholarly communication | 0.000 | 0.000 |
| Open science | 0.000 | 0.000 |
| Research integrity | 0.000 | 0.000 |
| Insufficient payload (model declined to judge) | 0.001 | 0.000 |
Machine scores (provisional)
The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.
Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.
score_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it