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Record W1994764615 · doi:10.1002/ejoc.200800522

Apralactone A and a New Stereochemical Class of Curvularins from the Marine Fungus <i>Curvularia</i> sp.

2008· article· en· W1994764615 on OpenAlex
Hendrik Greve, Peter J. Schupp, Ekaterina Eguereva, Stefan Kehraus, Gerhard Kelter, Armin Maier, Heinz‐Herbert Fiebig, Gabriele M. König

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

fundA Canadian funder is recorded on the work.
no affNo Canadian affiliation: this work is invisible to an affiliation-only frame.
No Canadian affiliation. An affiliation-only frame, the usual design, would never have seen this work. It is one of the works that make the case for inverting the frame.

Bibliographic record

VenueEuropean Journal of Organic Chemistry · 2008
Typearticle
Languageen
FieldMedicine
TopicMicrobial Natural Products and Biosynthesis
Canadian institutionsnot available
FundersNational Institute of General Medical SciencesIndependent Electricity System OperatorNational Cancer InstituteRheinische Friedrich-Wilhelms-Universität BonnBundesministerium für Bildung und Forschung
KeywordsChemistryStereochemistryFungusCurvulariaCytotoxic T cellStrain (injury)Marine fungiIn vitroBotanyPenicilliumBiologyBiochemistry

Abstract

fetched live from OpenAlex

Abstract Chemical investigations of the cytotoxic extract of the marine fungus Curvularia sp. (strain no. 768), isolated from the red alga Acanthophora spicifera , yielded the novel macrolide apralactone A ( 1 ), as well as the antipodes of curvularin macrolides 2 – 7 . Compound 8 , a dimeric curvularin was recognised as an artefact. The structures of 1 – 8 were elucidated by interpretation of their spectroscopic data (1D and 2D NMR, CD, MS, UV and IR). Apralactone A ( 1 ) is a 14‐membered phenyl acetic acid macrolactone, and the first such compound with a 4‐chromanone substructure. Compounds 1 , 2 , 4 , 5 and 6 were found to be cytotoxic towards human tumor cell lines with mean IC 50 values in the range of 1.25 to 30.06 μ M . (© Wiley‐VCH Verlag GmbH &amp; Co. KGaA, 69451 Weinheim, Germany, 2008)

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.001
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesInsufficient payload (model declined to judge)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.045
Threshold uncertainty score0.999

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.001
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.001
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.017
GPT teacher head0.204
Teacher spread0.186 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it