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Record W1995440483 · doi:10.1021/ja072269p

Smart Aptamers Facilitate Multi-Probe Affinity Analysis of Proteins with Ultra-Wide Dynamic Range of Measured Concentrations

2007· article· en· W1995440483 on OpenAlexaff
Andrei P. Drabovich, Victor Okhonin, Maxim V. Berezovski, Sergey N. Krylov

Bibliographic record

VenueJournal of the American Chemical Society · 2007
Typearticle
Languageen
FieldBiochemistry, Genetics and Molecular Biology
TopicAdvanced biosensing and bioanalysis techniques
Canadian institutionsYork University
Fundersnot available
KeywordsAptamerDynamic rangeChemistryCapillary electrophoresisWide dynamic rangeRange (aeronautics)Affinity electrophoresisBiophysicsNanotechnologyBiological systemAnalytical Chemistry (journal)ChromatographyAffinity chromatographyBiochemistryComputer scienceMaterials scienceMolecular biology

Abstract

fetched live from OpenAlex

Protein concentration can vary over several orders of magnitude in many physiological, pathological, and biotechnological processes. Studies of these processes require affinity analysis of proteins with a wide dynamic range of accurately measured concentrations. The wide dynamic range can be achieved with multiple affinity probes that bind the target with significantly different equilibrium constants ( K d ). Every probe in such a multi-probe affinity analysis is responsible for detection of the target in a range of concentrations around its K d value. A multi-probe affinity analysis of proteins has not become practical so far due to the lack of generic affinity probes with a wide range of K d and high selectivity. Kinetic capillary electrophoresis (KCE) has been recently proven to generate smart DNA aptamers with a wide range of predefined values of K d and high selectivity. Here, we demonstrate, for the first time, that such aptamers can facilitate multi-probe affinity analysis of a protein with an ultra-wide dynamic range of measured concentrations. Our results showed that a three-aptamer analysis had a concentration dynamic range of more than 4 orders of magnitude. To the best of our knowledge, this is the widest dynamic range ever reported for affinity analyses of proteins. Advantageously, protein concentration in a multi-aptamers analysis can be determined using a simple calibration-free approach. This work proves that the wide range of predefined binding parameters of smart aptamers can bring new capabilities to quantitative affinity analyses. The same feature of smart aptamers makes them potentially indispensable molecular tools in studies of intracellular processes.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.010
Threshold uncertainty score0.344

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.001
Bibliometrics0.0000.001
Science and technology studies0.0000.001
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.013
GPT teacher head0.269
Teacher spread0.256 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations56
Published2007
Admission routes1
Has abstractyes

Explore more

Same venueJournal of the American Chemical SocietySame topicAdvanced biosensing and bioanalysis techniquesFrench-language works237,207