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Record W2008827418 · doi:10.1063/1.2069519

Double sublimation system to deposit molecules from solid organic compounds onto a cryogenic substrate: Thymine on solid argon

2005· article· en· W2008827418 on OpenAlexafffund
Pierre L. Lévesque, M. Michaud, Léon Sanche

Bibliographic record

VenueReview of Scientific Instruments · 2005
Typearticle
Languageen
FieldEarth and Planetary Sciences
Topicnanoparticles nucleation surface interactions
Canadian institutionsUniversité de Sherbrooke
FundersCanadian Institutes of Health Research
KeywordsSublimation (psychology)Materials scienceInertInert gasArgonSubstrate (aquarium)Analytical Chemistry (journal)ChemistryComposite materialOrganic chemistry

Abstract

fetched live from OpenAlex

We report on the design, operation, and performance of a double sublimation system for the deposition of a submonolayer up to a few layers of a low-vapor pressure molecular solid compound onto a cryogenic substrate. The system consists of a primary oven (i.e., crucible type) to degas and first sublimate the compound onto the tip of a secondary oven (i.e., finger type), which is then used to transport the purified compound inside an analysis chamber and sublimate it just in front of the cryogenic substrate. The latter is kept at exactly the same position all the time, which is essential for experiments sensitive to target position. Besides, the negligible radiant heat transfer from the tip of the secondary oven allows operation in the presence of a cryogenic substrate consisting of an inert gas solid. The overall performance of the system is studied by EEL spectroscopy for thymine deposited onto a multilayer film of Ar used as an inert cryogenic substrate.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.001
Threshold uncertainty score0.004

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0010.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0010.001
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.020
GPT teacher head0.264
Teacher spread0.244 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations11
Published2005
Admission routes2
Has abstractyes

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Same venueReview of Scientific InstrumentsSame topicnanoparticles nucleation surface interactionsFrench-language works237,207