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Record W2010999859 · doi:10.1021/jp910643e

Assignment of the 6,6′-Dioxo-3,3′-biverdazyl Ground State by Using Broken Symmetry and Spectroscopy Oriented Configuration Interaction Techniques

2010· article· en· W2010999859 on OpenAlexaff
Saba M. Mattar, Hisham Dokainish

Bibliographic record

VenueThe Journal of Physical Chemistry A · 2010
Typearticle
Languageen
FieldMaterials Science
TopicMagnetism in coordination complexes
Canadian institutionsUniversity of New Brunswick
Fundersnot available
KeywordsSinglet stateGround stateDiradicalAntiferromagnetismConfiguration interactionSpectroscopyDihedral angleUnpaired electronChemistrySpin (aerodynamics)PhysicsElectron paramagnetic resonanceAtomic physicsCondensed matter physicsQuantum mechanicsExcited stateMoleculeHydrogen bond

Abstract

fetched live from OpenAlex

The singlet-triplet energy differences (DeltaE(ST)) and the Heisenberg-Dirac-van-Vleck exchange parameter (J) of 6,6'-dioxo-3,3'-biverdazyl (BVD) have been studied by hybrid density functional (HDF), broken symmetry (BS), and spectroscopy oriented configuration interaction (SORCI) methods. Energy surface scans as a function of the dihedral angle between the two verdazyl rings (phi(N2C3C3'N2')) have been performed. The BS computations predict an antiferromagnetic ground state. However, the diradical index (R(BS)) ranges from 97.5 to 99.9%, implying that the interactions between the two unpaired electrons are very weak. To calculate J and DeltaE(ST), the multireference character introduced by these weak spin-spin interactions must be taken into account. Consequently, multireference difference dedicated configuration interaction (MRDDCI) methods, as implemented in the SORCI procedure, are used. The in-plane pi (IPpi), out-of-plane pi (OPpi), and sigma configurations are included in the CI expansions in a balanced fashion. The OPpi-OPpi and OPpi-IPpi overlaps are the predominant factors that influence the J and DeltaE(ST) as a function of phi(N2C3C3'N2') and cause them to peak around 40 and 140 degrees. In these regions, the antiferromagnetic interactions are minimal, and the MRDDCI methods predict a triplet ground state. At phi(N2C3C3'N2') = 0, DeltaE(ST)[MRDDCI3(14,12)] is in excellent agreement with that of 1,1',5,5'-tetramethyl-6,6'-dioxo-3,3'-biverdazyl determined experimentally from electron paramagnetic resonance (EPR) spectroscopy and differs only by 2.3%. Furthermore, DeltaE(ST)[MRDDCI3(14,12)] is consistently smaller than J(Y) as the verdazyl rings rotate with respect to each other. This corroborates the theory that the HDF-BS technique increases the singlet-triplet energy gap and favors the singlet state. Because the SORCI method is specifically designed for large molecules, the present very good results open the way for the computation of the magnetic properties of larger molecules by the SORCI method. To the best of our knowledge, this is the first time that DeltaE(ST) has been computed by the MRDDCI3 method by utilizing such a large CI reference space for a molecule of this size.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.005
Threshold uncertainty score0.233

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.009
GPT teacher head0.272
Teacher spread0.263 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations8
Published2010
Admission routes1
Has abstractyes

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