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Record W2013371121 · doi:10.1088/0957-0233/18/5/017

Measurement of low concentration and nano-quantity hydrogen sulfide in aqueous solution: measurement mechanisms and limitations

2007· article· en· W2013371121 on OpenAlex
X C Wu, Ramaswami Sammynaiken, Wenjun Zhang, Dong Wu, Q. Yang, Wei Yang, Rui Wang

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.
fundA Canadian funder is recorded on the work.

Bibliographic record

VenueMeasurement Science and Technology · 2007
Typearticle
Languageen
FieldBiochemistry, Genetics and Molecular Biology
TopicSulfur Compounds in Biology
Canadian institutionsLakehead UniversityUniversity of Saskatchewan
FundersNatural Sciences and Engineering Research Council of Canada
KeywordsHydrogen sulfideRaman spectroscopyMicroscopeConfocalMaterials scienceRaman microscopeLaser scanningResolution (logic)LaserAqueous solutionAnalytical Chemistry (journal)Nano-MicroscopyNanotechnologyOpticsChemistrySulfurRaman scatteringChromatographyComputer science

Abstract

fetched live from OpenAlex

To measure hydrogen sulfide (H2S) level in biological samples in vivo on a real-time basis with high resolution is greatly needed for advancing our understanding of the biological role of H2S. Traditional H2S measurements usually need large tissue samples and complex procedures. However, H2S concentration is very low in human bodies and the tissue sample is limited for medical treatment purposes. There is a need to develop a new paradigm for the real-time measurement of a trace amount of hydrogen sulfide with a small amount of tissue samples or in vivo. We previously reported a method to measure low concentration H2S solution using carbon nanotubes and the fluorescence spectra of Raman and confocal laser scanning microscopes. We obtained that the measurement resolution with a confocal laser scanning microscope is higher than that with a Raman microscope; in particular, 10 µM concentration difference can be detected with a confocal laser scanning microscope. In this paper, we present the underlying mechanism and limitation of this method together with other traditional methods based on the theoretical analysis, which leads to the finding of further research on the measurement of low concentration and nano-quantity H2S solution.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.006
metaresearch head score (Gemma)0.002
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.018
Threshold uncertainty score0.675

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0060.002
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.001
Science and technology studies0.0000.001
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.038
GPT teacher head0.250
Teacher spread0.211 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it