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Record W2013463157 · doi:10.1139/v04-054

Spectroscopy of the XeC<sub>2</sub> molecule in xenon, argon, and krypton matrices

2004· article· en· W2013463157 on OpenAlexvenueno aff
Marcin Frankowski, A. M. Smith-Gicklhorn, V. E. Bondybey

Bibliographic record

VenueCanadian Journal of Chemistry · 2004
Typearticle
Languageen
FieldChemistry
TopicInorganic Fluorides and Related Compounds
Canadian institutionsnot available
FundersDeutsche Forschungsgemeinschaft
KeywordsChemistryKryptonXenonMoleculeMatrix isolationArgonSinglet stateGround stateInfrared spectroscopySpectral lineSpectroscopyAtomic physicsIonAnalytical Chemistry (journal)Excited statePhysics

Abstract

fetched live from OpenAlex

A self-igniting DC-electric discharge of C 2 H 2 in Xe (matrix gas) or C 2 H 2 and Xe in Ar or Kr (matrix gas) is used to produce and study the XeC 2 molecule in these various rare gases at 12 K. Unlike in Ar and Kr, the well-known electronic spectra of C 2 is completely absent in a Xe matrix. This together with annealing experiments in Ar matrices indicate that ground state Xe and C 2 react uniquely and without a barrier to form the XeC 2 molecule. The IR-active C-C stretch of this compound is found to be close to the C-C stretching frequency of the C 2 anion, in excellent agreement with our density functional theoretical (DFT) calculations, which yield a XeCC singlet species bent by 148.6° and with substantial charge separation approaching Xe + C 2 – and a notably short (2.107 Å) Xe—C bond. The spectra of the Xe– 13 C– 12 C, Xe– 12 C– 13 C, and Xe– 13 C– 13 C species are also obtained and the isotopic shifts are in excellent agreement with the DFT predictions, although not sufficient to distinguish a bent from a linear structure. Numerous broad absorptions centered near 423 nm (in Xe) are observed, which are clearly due to the XeC 2 molecule. Laser-induced fluorescence studies reveal a near-IR emission likely due to XeC 2 but not yet understood. Infrared spectra in the Xe matrix reveal also formation of the HXeCCH molecule.Key words: matrix-isolation spectroscopy, rare gas compounds, charge transfer compounds, xenon–carbon bonds.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.009
Threshold uncertainty score0.458

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.001
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.003
GPT teacher head0.170
Teacher spread0.167 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations13
Published2004
Admission routes1
Has abstractyes

Explore more

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