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Record W2016521268 · doi:10.1021/om000055+

Density Functional Study of Neutral Salicylaldiminato Nickel(II) Complexes as Olefin Polymerization Catalysts

2000· article· en· W2016521268 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.
fundA Canadian funder is recorded on the work.

Bibliographic record

VenueOrganometallics · 2000
Typearticle
Languageen
FieldChemistry
TopicOrganometallic Complex Synthesis and Catalysis
Canadian institutionsUniversity of Calgary
FundersNatural Sciences and Engineering Research Council of Canada
KeywordsChemistryCatalysisNickelOlefin fiberOlefin polymerizationPolymerizationPolymer chemistryPhotochemistryOrganic chemistryPolymer

Abstract

fetched live from OpenAlex

The recent discovery of the ability of salicylaldiminato Ni(II) complexes to promote ethylene polymerization creates a potential for a new class of olefin polymerization catalysts. The major advantage of this type of catalyst is that they produce a neutral active center and thereby avoid the ion-pairing problems encountered with the homogeneous single-site catalysts in current use. The present DFT study investigates the polymerization mechanism of these neutral complexes as well as the electronic and steric effects of various substituents on the catalyst backbone. The addition of electron-withdrawing or -releasing substituents on the 5 position of the salicylaldiminato ring was found to result in small changes in the energies of the reactions in the polymerization mechanism. This is most likely due to the substituents' remoteness from the active center. Changing the electronic nature of the donor atoms resulted in larger shifts in energy. Finally, bulky substituents such as 2,6-diisopropylphenyl and 9-anthracenyl groups were found to have the largest effect on the reaction barriers and enthalpies in a direction that should substantially increase catalyst activity.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow), Insufficient payload (model declined to judge)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.098
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0010.000
Bibliometrics0.0000.001
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0980.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.014
GPT teacher head0.222
Teacher spread0.208 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it