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Record W2025457303 · doi:10.1021/ic301311m

Ternary Arsenides A<sub>2</sub>Zn<sub>5</sub>As<sub>4</sub> (A = K, Rb): Zintl Phases Built from <i>Stellae Quadrangulae</i>

2012· article· en· W2025457303 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.

Bibliographic record

VenueInorganic Chemistry · 2012
Typearticle
Languageen
FieldMaterials Science
TopicIron-based superconductors research
Canadian institutionsUniversity of Alberta
Fundersnot available
KeywordsChemistryTernary operationTetrahedronAlkali metalCrystallographyStoichiometryStructure typeGroup (periodic table)Space groupCrystal structureBand gapX-ray crystallographyInorganic chemistryPhysical chemistryCondensed matter physicsDiffractionPhysics

Abstract

fetched live from OpenAlex

Stoichiometric reaction of the elements at high temperature yields the ternary arsenides K(2)Zn(5)As(4) (650 °C) and Rb(2)Zn(5)As(4) (600 °C). They adopt a new structure type (Pearson symbol oC44, space group Cmcm, Z = 4; a = 11.5758(5) Å, b = 7.0476(3) Å, c = 11.6352(5) Å for K(2)Zn(5)As(4); a = 11.6649(5) Å, b = 7.0953(3) Å, c = 11.7585(5) Å for Rb(2)Zn(5)As(4)) with a complex three-dimensional framework of linked ZnAs(4) tetrahedra generating large channels that are occupied by the alkali-metal cations. An alternative and useful way of describing the structure is through the use of stellae quadrangulae each consisting of four ZnAs(4) tetrahedra capping an empty central tetrahedron. These compounds are Zintl phases; band structure calculations on K(2)Zn(5)As(4) and Rb(2)Zn(5)As(4) indicate semiconducting behavior with a direct band gap of 0.4 eV.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.001
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow), Insufficient payload (model declined to judge)
Consensus categoriesInsufficient payload (model declined to judge)
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.008
Threshold uncertainty score0.999

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.001
Meta-epidemiology (narrow)0.0010.001
Meta-epidemiology (broad)0.0010.000
Bibliometrics0.0000.001
Science and technology studies0.0010.001
Scholarly communication0.0000.001
Open science0.0020.001
Research integrity0.0010.001
Insufficient payload (model declined to judge)0.0030.005

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.017
GPT teacher head0.253
Teacher spread0.237 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it