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Record W2029770669 · doi:10.1081/ss-120019406

Comparison of Two Methods to Recover Lysozyme from Reverse Micellar Phases

2003· article· en· W2029770669 on OpenAlexafffund
Youn‐Ok Shin, Martin Weber, Juan H. Vera

Bibliographic record

VenueSeparation Science and Technology · 2003
Typearticle
Languageen
FieldBiochemistry, Genetics and Molecular Biology
TopicProtein purification and stability
Canadian institutionsMcGill University
FundersNatural Sciences and Engineering Research Council of Canada
KeywordsLysozymeChemistryPulmonary surfactantChromatographyMicelleMicellar solutionsCationic polymerizationSolventAqueous solutionMicellar liquid chromatographyAcetonePhase (matter)Aqueous two-phase systemPrecipitationOrganic chemistryBiochemistry

Abstract

fetched live from OpenAlex

Two methods were tested to recover lysozyme from reverse micellar phases formed either with an anionic surfactant or with a cationic surfactant. The conventional back extraction method of contacting the protein-containing reverse micellar phase with a fresh aqueous phase, with pH and salt concentration adjustment, did not recover lysozyme from either reverse micellar phase. The lysozyme removed from the reverse micellar phase precipitated at the aqueous–organic interface. A solvent precipitation method using a polar organic solvent added to either lysozyme-containing reverse micellar phase, precipitated lysozyme as a solid, while the surfactant was solubilized in the polar solvent. Of the seven solvents tested, acetone recovered 70% of the original lysozyme from the anionic reverse micellar phase without loss of activity. No active lysozyme could be recovered from the cationic reverse micellar system. In this case, the lysozyme was denatured by the high pH required for the initial extraction into the reverse micellar phase.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.003
metaresearch head score (Gemma)0.006
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.003
Threshold uncertainty score0.015

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0030.006
Meta-epidemiology (narrow)0.0020.001
Meta-epidemiology (broad)0.0010.001
Bibliometrics0.0020.001
Science and technology studies0.0010.001
Scholarly communication0.0010.001
Open science0.0010.001
Research integrity0.0020.002
Insufficient payload (model declined to judge)0.0010.002

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.037
GPT teacher head0.447
Teacher spread0.410 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations13
Published2003
Admission routes2
Has abstractyes

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