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Record W2030332737 · doi:10.1180/0026461026620030

Description and crystal structure of bobkingite, a new mineral from New Cliffe Hill Quarry, Stanton-under-Bardon, Leicestershire, UK

2002· article· en· W2030332737 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.
fundA Canadian funder is recorded on the work.

Bibliographic record

VenueMineralogical Magazine · 2002
Typearticle
Languageen
FieldMaterials Science
TopicCrystal Structures and Properties
Canadian institutionsGeological Survey of CanadaCanadian Museum of NatureUniversity of Manitoba
FundersNational Research Council CanadaNatural Sciences and Engineering Research Council of CanadaCanada Research Chairs
KeywordsMohs scale of mineral hardnessMonoclinic crystal systemPleochroismCrystallographyMalachiteElectron microprobeCrystal structureMineralogyMaterials scienceChemistryCopperMetallurgy

Abstract

fetched live from OpenAlex

Abstract Bobkingite, ideally is a new mineral from the New Cliffe Hill Quarry, Stantonunder-Bardon, Leicestershire, England. It occurs as very thin (⩽5 µm) transparent plates up to 0.2 mm across, perched on a compact fibrous crust of malachite and crystalline azurite attached to massive cuprite. Crystals are tabular on {001} with dominant {001} and minor {100} and {110}. Bobkingite is a soft pale blue colour with a pale-blue streak, vitreous lustre and no observable fluorescence under ultraviolet light. It has perfect {001} and fair {100} cleavages, no observable parting, conchoidal fracture, and is brittle. Its Mohs' hardness is 3 and the calculated density is 3.254 g/cm 3 . Bobkingite is biaxial negative with α = 1.724(2), β = 1.745(2), γ = 1.750(2), 2V γmeas = 33(6)°, 2V calc = 52°, pleochroism distinct, X = very pale blue, Z = pale greenish blue, X ^ a = 22° (in β obtuse), Y = c, Z = b . Bobkingite is monoclinic, space group C 2/ m , unit-cell parameters (refined from powder data): a = 10.301(8), b = 6.758(3), c = 8.835(7)Å, β = 111.53(6)°, V = 572.1(7)Å 3 , Z = 2. The seven strongest lines in the X-ray powder-diffraction pattern are [ d (Å), I , ( hkl )]: 8.199, 100, (001); 5.502, 100, (110); 5.029, 40, ( 01); 2.883, 80, (310); 2.693, 40, ( 13); 2.263, 40, (113), ( 03); 2.188, 50, ( 23). Chemical analysis by electron microprobe and crystal-structure solution and refinement gave CuO 70.46, Cl 12.71, H 2 O 19.19, O≡Cl –2.87, sum 99.49 wt.%, where the amount of H 2 O was determined by crystal-structure analysis. The resulting empirical formula on the basis of 12 anions (including 8 (OH) and 2H 2 O) is Cu 4.99 Cl 2.02 O 10 H 12 . The crystal structure was solved by direct methods and refined to an R index of 2.6% for 638 observed reflections measured with X-rays on a single crystal. Three distinct (Cuϕ 6 ) (ϕ = unspecified anion) octahedra share edges to form a framework that is related to the structures of paratacamite and the Cu 2 (OH) 3 Cl polymorphs, atacamite and clinoatacamite. The mineral is named for Robert King, formerly of the Department of Geology, Leicester University, prominent mineral collector and founding member of the Russell Society. The mineral and its name have been approved by the Commission on New Minerals and Mineral Names of the International Mineralogical Association.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow), Insufficient payload (model declined to judge)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: none
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.923
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0010.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0100.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.038
GPT teacher head0.223
Teacher spread0.185 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it