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Record W2031503719 · doi:10.1021/ma034617n

Hydrogel Microspheres Formed by Complex Coacervation of Partially MPEG-Grafted Poly(styrene-<i>a</i><i>lt</i>-maleic anhydride) with PDADMAC and Cross-Linking with Polyamines

2003· article· en· W2031503719 on OpenAlexaff
Xiangchun Yin, Harald D. H. Stöver

Bibliographic record

VenueMacromolecules · 2003
Typearticle
Languageen
FieldBiochemistry, Genetics and Molecular Biology
TopicHydrogels: synthesis, properties, applications
Canadian institutionsMcMaster University
Fundersnot available
KeywordsCoacervatePolymer chemistryMaleic anhydridePolyelectrolyteStyreneCopolymerChemistryChitosanMaleic acidPoly(methacrylic acid)Materials scienceChemical engineeringMethacrylic acidOrganic chemistryPolymerChromatography

Abstract

fetched live from OpenAlex

Poly(styrene- alt -maleic anhydride) partially grafted with methoxy poly(ethylene glycol) (SMA- g -MPEG) was prepared by reacting poly(styrene- alt -maleic anhydride) with a substoichiometric amount of MPEG lithium alcoholate. Aqueous solutions of the resulting SMA- g -MPEG formed complex coacervates with poly(diallyldimethylammonium chloride) (PDADMAC). These phase-separated liquid polyelectrolyte complexes were subsequently cross-linked by the addition of two different polyamines to prepare cross-linked hydrogel microspheres. Chitosan served as an effective cross-linker at pH 7.0, while polyethylenimine (PEI) was used as cross-linker under basic conditions (pH 10.5). The resulting coacervate microspheres swelled with increasing salinity, which was attributed mainly due to the shielding of the electrostatic association within the polyelectrolyte complex. The morphology of the coacervate microspheres was investigated by environmental scanning electron microscopy.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.030
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.001
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.012
GPT teacher head0.234
Teacher spread0.222 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations34
Published2003
Admission routes1
Has abstractyes

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