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Record W2031995398 · doi:10.1021/om000486s

A Combined Density Functional and Molecular Dynamics Study on Ethylene Insertion into the Cp<sub>2</sub>ZrEt−MeB(C<sub>6</sub>F<sub>5</sub>)<sub>3</sub> Ion-Pair

2000· article· en· W2031995398 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.
fundA Canadian funder is recorded on the work.

Bibliographic record

VenueOrganometallics · 2000
Typearticle
Languageen
FieldChemistry
TopicOrganometallic Complex Synthesis and Catalysis
Canadian institutionsUniversity of Calgary
FundersNatural Sciences and Engineering Research Council of Canada
KeywordsChemistryCounterionEthyleneIonCrystallographyOlefin fiberDensity functional theoryMigratory insertionMoleculeAgostic interactionStereochemistryComputational chemistryMetalCatalysisOrganic chemistry

Abstract

fetched live from OpenAlex

Several aspects related to the insertion process of an ethylene molecule into the Zr−ethyl (Et) bond of the Cp 2 ZrEt−MeB(C 6 F 5 ) 3 contact ion-pair were examined by static density functional and first-principles molecular dynamic methods. The most stable conformer of this contact ion-pair can be described as having the anion coordinated to the Zr on the backside of the ethyl chain via a methyl bridge. This most stable conformation of Cp 2 ZrEt−MeB(C 6 F 5 ) 3 contained no agostic interactions with any of the hydrogen atoms on the ethyl chain. The insertion pathway studied considers the ethylene to approach the metal center of the contact ion-pair from the side opposite the anion. The ethyl chain rotates away from the olefin and the anion was pushed out of the coordination sphere of the zirconium before complexation occurs. The insertion occurs rapidly and apparently without significant barrier after successful complexation of the olefin. The behavior of the counterion after insertion was also examined. Considerations were given to an associative mechanism in which the counterion recombines with the catalyst to form a new contact ion-pair. Also considered was a dissociative mechanism in which the counterion continues to detach from the cation via the formation of an olefin-separated ion-pair. Either mechanism is a possibility depending on the conditions under which the polymerization is carried out.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow), Science and technology studies
Consensus categoriesMeta-epidemiology (narrow)
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.073
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.000
Meta-epidemiology (narrow)0.0020.002
Meta-epidemiology (broad)0.0020.001
Bibliometrics0.0010.002
Science and technology studies0.0010.001
Scholarly communication0.0010.001
Open science0.0010.001
Research integrity0.0010.001
Insufficient payload (model declined to judge)0.0010.001

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.008
GPT teacher head0.195
Teacher spread0.186 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it