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Record W2035795877 · doi:10.1021/la8033935

Modeling the Micellization Behavior of Mixed and Pure <i>n</i>-Alkyl-Maltosides

2009· article· en· W2035795877 on OpenAlexaff
Alekos Tsamaloukas, Andreas Beck, Heiko Heerklotz

Bibliographic record

VenueLangmuir · 2009
Typearticle
Languageen
FieldChemistry
TopicSurfactants and Colloidal Systems
Canadian institutionsUniversity of Toronto
Fundersnot available
KeywordsChemistryMicelleIsothermal titration calorimetryAlkylEnthalpyDynamic light scatteringAqueous solutionMethyleneHydrodynamic radiusCalorimetryPulmonary surfactantThermodynamicsThermodynamics of micellizationStatic light scatteringPhysical chemistryCritical micelle concentrationAnalytical Chemistry (journal)Organic chemistryMaterials scienceNanoparticle

Abstract

fetched live from OpenAlex

The micellization behavior of a series of n-alkyl-maltosides in aqueous solution was studied by isothermal titration calorimetry (ITC) and dynamic light scattering (DLS) at 25 degrees C. Demicellization experiments were conducted with single component micelles of octyl (OM), nonyl (NM), decyl (DM), undecyl (UM), and dodecyl (lauryl, LM) maltoside and binary mixtures of LM with OM, NM, DM and UM, respectively. A model was derived on the basis of the pseudophase approximation to fit the complete demicellization curves. It yielded good global fits of the curves obtained at different mixing ratios and ranging over >3 orders of magnitude in concentrations. It provides a quantitative explanation for the two-range coassociation behavior of the surfactant mixtures also in the absence of second critical micelle concentration (CMC) phenomena. The hydrodynamic radius, RH, of the mixed micelles was the average of that of the pure components as seen by noninvasive backscattering (NIBS) DLS. Methylene group contributions were constant for octyl through myristyl chains, amounting to -3.1 kJ/mol for the standard free energy and -1.8 kJ/mol for the enthalpy of micellization. RH increased by 0.25 nm per methylene.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Simulation or modeling · Consensus signal: Simulation or modeling
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.004
Threshold uncertainty score0.009

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.014
GPT teacher head0.224
Teacher spread0.211 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designSimulation or modeling
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations39
Published2009
Admission routes1
Has abstractyes

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