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Record W2038890159 · doi:10.1002/aic.11844

Structure and composition of CO<sub>2</sub>/H<sub>2</sub> and CO<sub>2</sub>/H<sub>2</sub>/C<sub>3</sub>H<sub>8</sub> hydrate in relation to simultaneous CO<sub>2</sub> capture and H<sub>2</sub> production

2009· article· en· W2038890159 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.
fundA Canadian funder is recorded on the work.

Bibliographic record

VenueAIChE Journal · 2009
Typearticle
Languageen
FieldEnvironmental Science
TopicMethane Hydrates and Related Phenomena
Canadian institutionsNational Research Council CanadaSteacie Institute for Molecular SciencesUniversity of British Columbia
FundersNatural Resources CanadaNatural Sciences and Engineering Research Council of CanadaCanadian Natural Resources Limited
KeywordsHydrateClathrate hydratePowder diffractionTernary operationRaman spectroscopyChemistryCrystal structureCrystallographyAnalytical Chemistry (journal)Chemical compositionInfrared spectroscopyX-ray crystallographyDiffractionMineralogyChromatographyOrganic chemistry

Abstract

fetched live from OpenAlex

Abstract Gas hydrates from a (40/60 mol %) CO 2 /H 2 mixture, and from a (38.2/59.2/2.6 mol %) CO 2 /H 2 /C 3 H 8 mixture, were synthesized using ice powder. The gas uptake curves were determined from pressure drop measurements and samples were analyzed using spectroscopic techniques to identify the structure and determine the cage occupancies. Powder X‐ray diffraction (PXRD) analysis at −110°C was used to determine the crystal structure. From the PXRD measurement it was found that the CO 2 /H 2 hydrate is structure I and shows a self‐preservation behavior similar to that of CO 2 hydrate. The ternary gas mixture was found to form pure structure II hydrate at 3.8 MPa. We have applied attenuated total reflection infrared spectroscopic analysis to measure the CO 2 distribution over the large and small cavities. 1 H MAS NMR and Raman were used to follow H 2 enclathration in the small cages of structure I, as well as structure II hydrate. © 2009 American Institute of Chemical Engineers AIChE J, 2009

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.006
metaresearch head score (Gemma)0.001
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow), Science and technology studies, Scholarly communication, Research integrity
Consensus categoriesMeta-epidemiology (narrow), Science and technology studies, Research integrity
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.053
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0060.001
Meta-epidemiology (narrow)0.0050.005
Meta-epidemiology (broad)0.0050.001
Bibliometrics0.0030.005
Science and technology studies0.0040.003
Scholarly communication0.0020.005
Open science0.0020.001
Research integrity0.0050.009
Insufficient payload (model declined to judge)0.0000.001

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.007
GPT teacher head0.217
Teacher spread0.211 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it