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Record W2042111715 · doi:10.1021/cm060407o

Toward the Development of New Textile/Plastic Electrochromic Cells Using Triphenylamine-Based Copolymers

2006· article· en· W2042111715 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.

Bibliographic record

VenueChemistry of Materials · 2006
Typearticle
Languageen
FieldMaterials Science
TopicConducting polymers and applications
Canadian institutionsUniversité LavalDefence Research and Development Canada
Fundersnot available
KeywordsElectrochromismTriphenylamineMaterials scienceCopolymerPolymerElectrochromic devicesPolymer chemistryElectrochemistryGlass transitionChemical engineeringChemistryComposite materialElectrodePhysical chemistry

Abstract

fetched live from OpenAlex

We report the preparation and characterization of new electrochromic polymers containing a 4-butyltriphenylamine (BuTPA) unit on the main chain. All polymers were obtained through the Suzuki−Miyaura cross-coupling reaction between 4-butyl- N, N -bis((4,4,5,5-tetramethyl-1,3,2-dioxaborolan-4-phenyl)aniline) and several aryl dibromide molecules to modulate the electronic properties of the resulting copolymers. 2,5-Dibromothiophene, 2,5-dibromo(3,4-ethylenedioxythiophene), 3,6-dibromo- N -octylcarbazole, bis(6-bromo- N -octylcarbazol-3-yl), and 2,7-dibromo-3,6-dimethoxy-9,9-dihexylfluorene were used as comonomers and led to five new copolymers, PT(BuTPA), PE(BuTPA), PC(BuTPA), PCC(BuTPA), and PF(BuTPA). These polymers are readily soluble in many common organic solvents, which make them suitable for spray-coating film deposition. Electrochromic cells with the following configuration were assembled: ITO-coated glass or plastic/electrochromic polymer/gel electrolyte/ITO-coated glass or plastic or conducting textile. These copolymers exhibit good optical and electrochemical properties for military camouflage needs with color transition from pale yellow to green, transparent to khaki, or pale green to reddish-brown. Electrochemistry, spectroelectrochemistry, and colorimetric measurements of the devices were examined.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesInsufficient payload (model declined to judge)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.003
Threshold uncertainty score0.999

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.028
GPT teacher head0.249
Teacher spread0.222 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it