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USE OF A SINGLE-SOURCE MIXED-METAL PRECURSOR FOR THE PHOTODEPOSITION OF Pd/Ni OXIDES THIN FILMS

2002· article· es· W2045925792 on OpenAlexaff
G.E. Buono-Core, M. Tejos, G. Cabello, Fernando Arós, R. H. HILL

Bibliographic record

VenueBoletín de la Sociedad Chilena de Química · 2002
Typearticle
Languagees
FieldChemistry
TopicPhotochemistry and Electron Transfer Studies
Canadian institutionsSimon Fraser University
Fundersnot available
KeywordsMetalMaterials scienceX-ray photoelectron spectroscopyNon-blocking I/OMineralogyNuclear chemistryPhysicsChemistryMetallurgy

Abstract

fetched live from OpenAlex

Irradiation of thin films of a polyketonate Pd/Ni heteronuclear complex, PdNi(DBA)2 [DBA = dibenzoylacetone)], produced uniform films containing Pd and Ni as shown by EDAX analysis. The X-ray powder diffraction spectrum showed peaks associated with elemental Pd and NiO. The morphology of the films was examined by SEM measurements showing a uniform granular surface with particle sizes of 100 nm or less. The XPS results show that the ratio of Pd/Ni (1:17) present in the film does reflect the stoichiometry in the starting complex. The large amount of carbon (52 %) detected on the surface of the film may be due to the presence of phenyl rings in the precursor complex.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.008
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0010.000
Meta-epidemiology (broad)0.0010.001
Bibliometrics0.0000.000
Science and technology studies0.0000.001
Scholarly communication0.0000.000
Open science0.0010.000
Research integrity0.0010.001
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.018
GPT teacher head0.233
Teacher spread0.215 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations6
Published2002
Admission routes1
Has abstractyes

Explore more

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