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Record W2047441588 · doi:10.1021/jp310013z

Electronic Structure of Graphdiyne Probed by X-ray Absorption Spectroscopy and Scanning Transmission X-ray Microscopy

2013· article· en· W2047441588 on OpenAlexaff
Jun Zhong, Jian Wang, Jigang Zhou, Baohua Mao, Changhai Liu, Hui-Biao Liu, Yuliang Li, Tsun‐Kong Sham, Sui‐Dong Wang

Bibliographic record

VenueThe Journal of Physical Chemistry C · 2013
Typearticle
Languageen
FieldMaterials Science
TopicGraphene research and applications
Canadian institutionsCanadian Light Source (Canada)University of SaskatchewanWestern University
Fundersnot available
KeywordsAnnealing (glass)X-rayAbsorption spectroscopyNitrogenTriple bondSpectroscopyAbsorption (acoustics)Materials scienceX-ray absorption spectroscopyCarbon fibersX-ray photoelectron spectroscopyAnalytical Chemistry (journal)ChemistryCrystallographyDouble bondOpticsComposite numberChemical engineeringComposite materialOrganic chemistryPolymer chemistryPhysics

Abstract

fetched live from OpenAlex

The electronic structure of graphdiyne exposed to air is investigated utilizing X-ray absorption spectroscopy and scanning transmission X-ray microscopy. It is found that carbon–carbon triple bonds at defect sites in graphdiyne have been changed to double bonds after 3 months in air. The experimental results reveal the existence of oxygen and nitrogen functional groups and indicate that the oxidation takes place throughout the aged graphdiyne while the nitrogen contamination is mainly on its surface. Buckling of the aged graphdiyne is observed, resulting from bond length change due to the opening of triple bonds. It is also shown that annealing at a high temperature such as 800 °C may remove most of the functional groups in the aged graphdiyne.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.005
Threshold uncertainty score0.269

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.004
GPT teacher head0.248
Teacher spread0.244 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations86
Published2013
Admission routes1
Has abstractyes

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